C₂₅H₃₁NO₇

Base Information

Chemical Name:C₂₅H₃₁NO₇
CAS No.:1359021-89-8
Molecular Formula:C₂₅H₃₁NO₇
Molecular Weight:457.524
Hs Code.:

C<sub>25</sub>H<sub>31</sub>NO<sub>7</sub>

Synonyms:C₂₅H₃₁NO₇

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Chemical Property of C₂₅H₃₁NO₇

Chemical Property:

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Technology Process of C₂₅H₃₁NO₇

There total 14 articles about C₂₅H₃₁NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50868-73-0
2-methoxy-6-methylbenzeneamine

: 1359021-89-8
C₂₅H₃₁NO₇

Guidance literature:: Multi-step reaction with 14 steps

1.1: bromine; acetic acid / methanol / 2 h / 20 °C / Cooling with ice

2.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

2.2: 4 h / 0 - 50 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

3.2: 1 h / 20 °C

4.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

4.2: pH 1

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

6.1: triethylamine / dmap / 1 h / 20 °C

7.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

7.2: 0.33 h / 20 °C

8.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 17 h / 0 - 20 °C

8.2: 0.33 h / 20 °C

9.1: potassium carbonate / acetone / 2 h / Reflux

10.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -100 °C

10.2: 3 h / -100 - -78 °C

10.3: -78 °C

11.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C

12.1: hydrogen / palladium on activated carbon / methanol / 2 h / 760.05 Torr / Sealed vessel

13.1: acetic acid; triethylamine / 1,2-dichloro-ethane / 2 h / 20 °C

13.2: 2 h / 20 °C

14.1: dmap / dichloromethane / 1 h / 20 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; [bis(acetoxy)iodo]benzene; hydrogen; bromine; boron tribromide; diisobutylaluminium hydride; potassium carbonate; acetic acid; triethylamine; sodium nitrite; dmap; palladium on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; acetone; toluene; tert-butyl alcohol;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1359021-89-8
C₂₅H₃₁NO₇

Guidance literature:: Multi-step reaction with 12 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

1.2: 1 h / 20 °C

2.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: triethylamine / dmap / 1 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

5.2: 0.33 h / 20 °C

6.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 17 h / 0 - 20 °C

6.2: 0.33 h / 20 °C

7.1: potassium carbonate / acetone / 2 h / Reflux

8.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -100 °C

8.2: 3 h / -100 - -78 °C

8.3: -78 °C

9.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C

10.1: hydrogen / palladium on activated carbon / methanol / 2 h / 760.05 Torr / Sealed vessel

11.1: acetic acid; triethylamine / 1,2-dichloro-ethane / 2 h / 20 °C

11.2: 2 h / 20 °C

12.1: dmap / dichloromethane / 1 h / 20 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; [bis(acetoxy)iodo]benzene; hydrogen; boron tribromide; diisobutylaluminium hydride; potassium carbonate; acetic acid; triethylamine; dmap; palladium on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; acetone; toluene; tert-butyl alcohol;

Reference yield:

: 877149-08-1
4-bromo-2-methoxy-6-methyl-benzoic acid

: 1359021-89-8
C₂₅H₃₁NO₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

2.1: triethylamine / dmap / 1 h / 20 °C

3.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

3.2: 0.33 h / 20 °C

4.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 17 h / 0 - 20 °C

4.2: 0.33 h / 20 °C

5.1: potassium carbonate / acetone / 2 h / Reflux

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -100 °C

6.2: 3 h / -100 - -78 °C

6.3: -78 °C

7.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C

8.1: hydrogen / palladium on activated carbon / methanol / 2 h / 760.05 Torr / Sealed vessel

9.1: acetic acid; triethylamine / 1,2-dichloro-ethane / 2 h / 20 °C

9.2: 2 h / 20 °C

10.1: dmap / dichloromethane / 1 h / 20 °C

With hydrogenchloride; n-butyllithium; oxalyl dichloride; [bis(acetoxy)iodo]benzene; hydrogen; boron tribromide; potassium carbonate; acetic acid; triethylamine; dmap; palladium on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; acetone;