4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranose

Base Information

Chemical Name:4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranose
CAS No.:171412-27-4
Molecular Formula:C₅₆H₅₅NO₁₄
Molecular Weight:966.051
Hs Code.:

Synonyms:4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranose

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Chemical Property of 4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranose

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Technology Process of 4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranose

There total 12 articles about 4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 142329-99-5
4-methoxybenzyl O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-(1<*>4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 171412-27-4
4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranose

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;
DOI:10.1246/cl.1992.707

Reference yield:

: 142329-98-4
4-methoxybenzyl O-<3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-D-arabino-hexopyranosyl>-(1<*>4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 171412-27-4
4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BH₃*THF / 1.) THF, from -10 deg C to RT, 2.5 h, 2.) THF, methanol, RT, 1 h

2: DDQ / CH₂Cl₂; H₂O / Ambient temperature

With borane-THF; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;
DOI:10.1246/bcsj.68.2401

Reference yield:

: 142329-95-1
p-methoxybenzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 171412-27-4
4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) molecular sieves 3A, silver carbonate, silver zeolite / 1.) CH₂Cl₂, RT, 1 h, 2.) CH₂Cl₂, RT, 2 d

2: 1.) BH₃*THF / 1.) THF, from -10 deg C to RT, 2.5 h, 2.) THF, methanol, RT, 1 h

3: DDQ / CH₂Cl₂; H₂O / Ambient temperature

With borane-THF; 3 A molecular sieve; silver zeolite; silver carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;
DOI:10.1246/bcsj.68.2401