p-methoxybenzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxybenzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:142329-95-1
Molecular Formula:C₃₅H₃₈O₇
Molecular Weight:570.683
Hs Code.:

Synonyms:p-methoxybenzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of p-methoxybenzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of p-methoxybenzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 6 articles about p-methoxybenzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 142329-95-1
p-methoxybenzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / p-toluenesulfonic acid / dimethylformamide / 1 h / 60 °C

2: 1.) NaH / 1.) DMF, RT, 0.5 h, 2.) DMF, RT, overnight

3: 83 percent / molecular sieves 3A, sodium cyanotrihydroborate, HCl / diethyl ether / 0.17 h / 0 °C

With hydrogenchloride; 3 A molecular sieve; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.68.2401

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 142329-95-1
p-methoxybenzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / molecular sieves 3A, iodine, silver carbonate / diethyl ether / 24 h / Ambient temperature

2: 85 percent / sodium methoxide / methanol / 1 h / Ambient temperature

3: 77 percent / p-toluenesulfonic acid / dimethylformamide / 1 h / 60 °C

4: 1.) NaH / 1.) DMF, RT, 0.5 h, 2.) DMF, RT, overnight

5: 83 percent / molecular sieves 3A, sodium cyanotrihydroborate, HCl / diethyl ether / 0.17 h / 0 °C

With hydrogenchloride; 3 A molecular sieve; iodine; sodium methylate; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; silver carbonate; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.68.2401

Reference yield:

: 81381-72-8
(4-methoxyphenyl)methyl-β-D-glucopyranoside

: 142329-95-1
p-methoxybenzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / p-toluenesulfonic acid / dimethylformamide / 1 h / 60 °C

2: 1.) NaH / 1.) DMF, RT, 0.5 h, 2.) DMF, RT, overnight

3: 83 percent / molecular sieves 3A, sodium cyanotrihydroborate, HCl / diethyl ether / 0.17 h / 0 °C

With hydrogenchloride; 3 A molecular sieve; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.68.2401