phenylphosphan

Base Information

• Chemical Name: phenylphosphan
• CAS No.: 109152-83-2
• Molecular Formula: C₁₃H₂₅PSi₂
• Molecular Weight: 268.486

Synonyms:phenylphosphan

Chemical Property of phenylphosphan

Chemical Property:

Purity/Quality:

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Technology Process of phenylphosphan

There total 2 articles about phenylphosphan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

phenylphosphine (78928-41-3) → phenylphosphan (109152-83-2) + pentaphenylcyclopentaphosphane (3376-52-1)

Guidance literature:

With Natrium-phenylphosphid; diphenylphosphane; In tetrahydrofuran; at 25 ℃;

Reference yield:

{(Me3Si)2CH}(Ph)PCl (106112-93-0) → phenylphosphan (109152-83-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Inert atmosphere; Reflux;

DOI:10.1021/ic1003534

Reference yield: 63.0%

dimethylsulfide borane complex (13292-87-0) + phenylphosphan (109152-83-2) → C13H28BPSi2 (1418274-98-2)

Guidance literature:

In tetrahydrofuran; for 1h; Inert atmosphere; Schlenk technique;

DOI:10.1021/ic302205b

upstream raw materials:

phenylphosphine

{(Me₃Si)2CH}(Ph)PCl

Downstream raw materials:

C₁₃H₂₈BPSi₂

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