9-benzyloxy-10-methoxy-7H-4,5,12,12a-tetahydrobenzothieno<2,3-a>quinolizine

Base Information

Chemical Name:9-benzyloxy-10-methoxy-7H-4,5,12,12a-tetahydrobenzothieno<2,3-a>quinolizine
CAS No.:688301-90-8
Molecular Formula:C₂₃H₂₃NO₂S
Molecular Weight:377.507
Hs Code.:

9-benzyloxy-10-methoxy-7H-4,5,12,12a-tetahydrobenzo<g>thieno<2,3-a>quinolizine

Synonyms:9-benzyloxy-10-methoxy-7H-4,5,12,12a-tetahydrobenzothieno<2,3-a>quinolizine

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Chemical Property of 9-benzyloxy-10-methoxy-7H-4,5,12,12a-tetahydrobenzothieno<2,3-a>quinolizine

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Technology Process of 9-benzyloxy-10-methoxy-7H-4,5,12,12a-tetahydrobenzothieno<2,3-a>quinolizine

There total 7 articles about 9-benzyloxy-10-methoxy-7H-4,5,12,12a-tetahydrobenzothieno<2,3-a>quinolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 781565-01-3
7-(4'-benzyloxy-3'-methoxybenzyl)-4,5,6,7-tetrathieno<2,3-c>pyridine

: 688301-90-8
9-benzyloxy-10-methoxy-7H-4,5,12,12a-tetahydrobenzothieno<2,3-a>quinolizine

Guidance literature:: In acetic acid; for 1h; Heating;

Reference yield:

: 59311-67-0
2-(3-thienyl)ethylamine

: 688301-90-8
9-benzyloxy-10-methoxy-7H-4,5,12,12a-tetahydrobenzothieno<2,3-a>quinolizine

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / 2 h / Heating

2: PCl₅ / CHCl₃ / 10 h / Ambient temperature

3: 87 percent / NaBH₄ / methanol

4: 83 percent / acetic acid / 1 h / Heating

With sodium tetrahydroborate; phosphorus pentachloride; In methanol; chloroform; acetic acid;

Reference yield:

: 29973-91-9
4-benzyloxy-3-methoxyphenylacetic acid

: 688301-90-8
9-benzyloxy-10-methoxy-7H-4,5,12,12a-tetahydrobenzothieno<2,3-a>quinolizine

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / 2 h / Heating

2: PCl₅ / CHCl₃ / 10 h / Ambient temperature

3: 87 percent / NaBH₄ / methanol

4: 83 percent / acetic acid / 1 h / Heating

With sodium tetrahydroborate; phosphorus pentachloride; In methanol; chloroform; acetic acid;