O-(2'-cyano-2-biphenylylcarbonyl)-9,10-phenathrenequinone oxime

Base Information

• Chemical Name: O-(2'-cyano-2-biphenylylcarbonyl)-9,10-phenathrenequinone oxime
• CAS No.: 120007-29-6
• Molecular Formula: C₂₈H₁₆N₂O₃
• Molecular Weight: 428.447
• Mol file: 120007-29-6.mol

Synonyms:O-(2'-cyano-2-biphenylylcarbonyl)-9,10-phenathrenequinone oxime

Chemical Property of O-(2'-cyano-2-biphenylylcarbonyl)-9,10-phenathrenequinone oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of O-(2'-cyano-2-biphenylylcarbonyl)-9,10-phenathrenequinone oxime

There total 2 articles about O-(2'-cyano-2-biphenylylcarbonyl)-9,10-phenathrenequinone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.6%

phenanthrene-9,10-dione oxime (14140-04-6) + 2'-cyano-2-biphenylcarbonyl chloride (120007-30-9) → O-(2'-cyano-2-biphenylylcarbonyl)-9,10-phenathrenequinone oxime (120007-29-6)

Guidance literature:

With pyridine; In toluene; for 30h; Heating;

Reference yield: 55.4%

phenanthrene-9,10-dione oxime (14140-04-6) → O-(2'-cyano-2-biphenylylcarbonyl)-9,10-phenathrenequinone oxime (120007-29-6)

Guidance literature:

With pyridine; p-toluenesulfonyl chloride; In toluene; for 0.5h; Heating;

Reference yield: 87.2%

O-(2'-cyano-2-biphenylylcarbonyl)-9,10-phenathrenequinone oxime (120007-29-6) → 2'-cyano-[1,1'-biphenyl]-2-carboxylic acid (57743-13-2)

Guidance literature:

With calcium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; water; p-toluenesulfonyl chloride; In toluene; for 2h; Heating;

upstream raw materials:

phenanthrene-9,10-dione oxime

2'-cyano-2-biphenylcarbonyl chloride

Downstream raw materials:

2'-cyano-[1,1'-biphenyl]-2-carboxylic acid