benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside

Base Information

Chemical Name:benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside
CAS No.:1350934-15-4
Molecular Formula:C₃₄H₃₄O₄S
Molecular Weight:538.708
Hs Code.:

Synonyms:benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside

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Chemical Property of benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside

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Technology Process of benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside

There total 4 articles about benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350934-06-3
1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-(phenylthiomethyl)-D-lyxo-hex-1-enitol

: benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside

: 1350934-15-4
benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside

Guidance literature:: With indium(III) chloride; In dichloromethane; at 30 ℃; for 1h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.122

Reference yield:

: 1092103-60-0
1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol

: 108-98-5
thiophenol

: benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside

: 1350934-15-4
benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: indium(III) chloride / acetonitrile / 0.25 h / 0 °C / Inert atmosphere

2: indium(III) chloride / dichloromethane / 1 h / 30 °C / Inert atmosphere

With indium(III) chloride; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2011.09.122

Reference yield:

: 1092103-65-5
1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-benzyloxymethyl-D-lyxo-hex-1-enitol

: 108-98-5
thiophenol

: benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside

: 1350934-15-4
benzyl 4,6-di-O-benzyl-2,3-dideoxy-2-C-(phenylthiomethyl)-D-threo-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: indium(III) chloride / acetonitrile / 0.25 h / 0 °C / Inert atmosphere

2: indium(III) chloride / dichloromethane / 1 h / 30 °C / Inert atmosphere

With indium(III) chloride; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2011.09.122