1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol

Base Information

Chemical Name:1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol
CAS No.:1092103-60-0
Molecular Formula:C₂₉H₃₂O₅
Molecular Weight:460.57
Hs Code.:

Synonyms:1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol

Suppliers and Price of 1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol

There total 1 articles about 1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 153496-00-5
1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-hydroxymethyl-D-lyxo-hex-1-enitol

: 74-88-4
methyl iodide

: 1092103-60-0
1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol

Guidance literature:: 1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-hydroxymethyl-D-lyxo-hex-1-enitol; With sodium hydride; In N,N-dimethyl-formamide; paraffin oil; at 0 ℃; for 0.0833333h;

methyl iodide; In N,N-dimethyl-formamide; paraffin oil; at 20 ℃; for 4h;
DOI:10.1002/ejoc.200800453

Reference yield: 88.0%

: 1092103-60-0
1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol

: 153081-98-2
methyl 3,4,6-tri-Obenzyl-2-deoxy-2-C-methylene-α-D-lyxo-hexopyranoside

Guidance literature:: With indium(III) chloride; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1002/ejoc.200800453

Reference yield: 62.0%

: 1092103-60-0
1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-methoxymethyl-D-lyxo-hex-1-enitol

: 108-98-5
thiophenol

: 1350934-06-3
1,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-C-(phenylthiomethyl)-D-lyxo-hex-1-enitol

: C₃₄H₃₄O₄S

Guidance literature:: With indium(III) chloride; In acetonitrile; at 0 ℃; for 0.25h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.122