3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid

Base Information

Chemical Name:3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid
CAS No.:420834-18-0
Molecular Formula:C₁₈H₂₀Cl₃NO₅
Molecular Weight:436.719
Hs Code.:

Synonyms:3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid

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Chemical Property of 3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid

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Technology Process of 3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid

There total 4 articles about 3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 420834-16-8
3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester

: 420834-18-0
3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid

Guidance literature:: 3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester; With lithium hydroxide; In methanol; at 20 ℃; for 0.5h;

With hydrogenchloride; In water;

Reference yield:

: 132201-32-2,161453-08-3,949459-75-0,521059-43-8
(2R,3S)-3-phenylisoserine hydrochloride

: 420834-18-0
3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / SOCl₂ / 0 °C

2: NaHCO₃ / CH₂Cl₂

3: p-TsOH / toluene / 110 °C

4: LiOH / methanol

With lithium hydroxide; thionyl chloride; sodium hydrogencarbonate; toluene-4-sulfonic acid; In methanol; dichloromethane; toluene;

Reference yield:

: methyl (2R,3S)-3-phenylisoserinate hydrochloride

: 420834-18-0
3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃ / CH₂Cl₂

2: p-TsOH / toluene / 110 °C

3: LiOH / methanol

With lithium hydroxide; sodium hydrogencarbonate; toluene-4-sulfonic acid; In methanol; dichloromethane; toluene;