3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester

Base Information

Chemical Name:3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester
CAS No.:420834-16-8
Molecular Formula:C₁₉H₂₂Cl₃NO₅
Molecular Weight:450.746
Hs Code.:

Synonyms:3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester

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Chemical Property of 3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester

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Technology Process of 3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester

There total 3 articles about 3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 933-40-4
cycloxexanone dimethyl ketal

: 157425-30-4
N-2,2,2-trichloroethoxycarbonyl phenylisoserine methyl ester

: 420834-16-8
3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 120 ℃; for 3h;

Reference yield:

: 132201-32-2,161453-08-3,949459-75-0,521059-43-8
(2R,3S)-3-phenylisoserine hydrochloride

: 420834-16-8
3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / SOCl₂ / 0 °C

2: NaHCO₃ / CH₂Cl₂

3: p-TsOH / toluene / 110 °C

With thionyl chloride; sodium hydrogencarbonate; toluene-4-sulfonic acid; In dichloromethane; toluene;

Reference yield:

: methyl (2R,3S)-3-phenylisoserinate hydrochloride

: 420834-16-8
3-(2,2,2-trichloroethoxycarbonyl)-2-cyclohexyl-4-phenyl-5-oxazolidinecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / CH₂Cl₂

2: p-TsOH / toluene / 110 °C

With sodium hydrogencarbonate; toluene-4-sulfonic acid; In dichloromethane; toluene;