1-<2-(1-benzyloxy-1-methylethyl)phenyl>-3,3-dimethyl-1-phenyl-3H-2,1-benzoxaphospholium bromide

Base Information

Chemical Name:1-<2-(1-benzyloxy-1-methylethyl)phenyl>-3,3-dimethyl-1-phenyl-3H-2,1-benzoxaphospholium bromide
CAS No.:82123-52-2
Molecular Formula:Br*C₃₁H₃₂O₂P
Molecular Weight:547.472
Hs Code.:

Synonyms:1-<2-(1-benzyloxy-1-methylethyl)phenyl>-3,3-dimethyl-1-phenyl-3H-2,1-benzoxaphospholium bromide

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Chemical Property of 1-<2-(1-benzyloxy-1-methylethyl)phenyl>-3,3-dimethyl-1-phenyl-3H-2,1-benzoxaphospholium bromide

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Technology Process of 1-<2-(1-benzyloxy-1-methylethyl)phenyl>-3,3-dimethyl-1-phenyl-3H-2,1-benzoxaphospholium bromide

There total 3 articles about 1-<2-(1-benzyloxy-1-methylethyl)phenyl>-3,3-dimethyl-1-phenyl-3H-2,1-benzoxaphospholium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-44-7
benzyl chloride

: 82123-52-2
1-<2-(1-benzyloxy-1-methylethyl)phenyl>-3,3-dimethyl-1-phenyl-3H-2,1-benzoxaphospholium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / potassium iodide, sodium hydride / 11 h / 95 °C

2: 1.) magnesium shavings, 1,2-dibromoethane / 1.) THF, reflux; 2.) THF, reflux, 1 h

3: 70 percent / Br₂ / CHCl₃; CCl₄

With bromine; sodium hydride; magnesium; ethylene dibromide; potassium iodide; In tetrachloromethane; chloroform;

Reference yield:

: 82123-47-5
benzyl-1-(2-bromophenyl)-1-methylethyl ether

: 82123-52-2
1-<2-(1-benzyloxy-1-methylethyl)phenyl>-3,3-dimethyl-1-phenyl-3H-2,1-benzoxaphospholium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) magnesium shavings, 1,2-dibromoethane / 1.) THF, reflux; 2.) THF, reflux, 1 h

2: 70 percent / Br₂ / CHCl₃; CCl₄

With bromine; magnesium; ethylene dibromide; In tetrachloromethane; chloroform;

Reference yield:

: 7073-69-0
2-(2-bromophenyl)propanol

: 82123-52-2
1-<2-(1-benzyloxy-1-methylethyl)phenyl>-3,3-dimethyl-1-phenyl-3H-2,1-benzoxaphospholium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / potassium iodide, sodium hydride / 11 h / 95 °C

2: 1.) magnesium shavings, 1,2-dibromoethane / 1.) THF, reflux; 2.) THF, reflux, 1 h

3: 70 percent / Br₂ / CHCl₃; CCl₄

With bromine; sodium hydride; magnesium; ethylene dibromide; potassium iodide; In tetrachloromethane; chloroform;