benzyl-1-(2-bromophenyl)-1-methylethyl ether

Base Information

• Chemical Name: benzyl-1-(2-bromophenyl)-1-methylethyl ether
• CAS No.: 82123-47-5
• Molecular Formula: C₁₆H₁₇BrO
• Molecular Weight: 305.214
• Mol file: 82123-47-5.mol

Synonyms:benzyl-1-(2-bromophenyl)-1-methylethyl ether

Chemical Property of benzyl-1-(2-bromophenyl)-1-methylethyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of benzyl-1-(2-bromophenyl)-1-methylethyl ether

There total 1 articles about benzyl-1-(2-bromophenyl)-1-methylethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

benzyl chloride (100-44-7) + 2-(2-bromophenyl)propanol (7073-69-0) → benzyl-1-(2-bromophenyl)-1-methylethyl ether (82123-47-5)

Guidance literature:

With sodium hydride; potassium iodide; at 95 ℃; for 11h;

Reference yield:

benzyl-1-(2-bromophenyl)-1-methylethyl ether (82123-47-5) → benzyl bromide (100-39-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) magnesium shavings, 1,2-dibromoethane / 1.) THF, reflux; 2.) THF, reflux, 1 h

2: 70 percent / Br₂ / CHCl₃; CCl₄

3: 0.17 h / 100 °C

With bromine; magnesium; ethylene dibromide; In tetrachloromethane; chloroform;

Reference yield:

benzyl-1-(2-bromophenyl)-1-methylethyl ether (82123-47-5) → 2-(1-hydroxy-1-methylethyl)phenyl(diphenyl)phosphine oxide (80750-50-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) Mg, 1,2-dibromoethane / 1.) THF, reflux; 2.) THF, reflux, 1 h

2: 73 percent / bromine / CCl₄; diethyl ether

3: sodium hydrogen carbonate, bromine / CHCl₃

With bromine; sodium hydrogencarbonate; magnesium; ethylene dibromide; In tetrachloromethane; diethyl ether; chloroform;

upstream raw materials:

benzyl chloride

2-(2-bromophenyl)propanol

Downstream raw materials:

bis<2-(1-methyl-1-benzyloxyethyl)phenyl>phenylphosphine

diphenyl-2-(1-methyl-1-benzyloxyethyl)phenylphosphine

3,3,3',3'-tetramethyl-1-phenyl-1,1'-spirobi<3H-2,1-benzoxaphosphole>

benzyl bromide

Refernces