Technology Process of C25H30N4O4Si
There total 5 articles about C25H30N4O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
tetrahydrofuran;
at 60 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; 1,2-dimethoxyethane / 16 h / 100 °C / Inert atmosphere
2.1: caesium carbonate / N,N-dimethyl-formamide / 0.33 h / Inert atmosphere
2.2: 2 h / 60 °C / Inert atmosphere
3.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h
4.1: tetrahydrofuran / 4 h / 60 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; hydrogen; sodium carbonate; caesium carbonate;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: caesium carbonate / N,N-dimethyl-formamide / 0.33 h / Inert atmosphere
1.2: 2 h / 60 °C / Inert atmosphere
2.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h
3.1: tetrahydrofuran / 4 h / 60 °C / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; caesium carbonate;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;