1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-amino-6''-deoxy-kanamycin A

Base Information

Chemical Name:1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-amino-6''-deoxy-kanamycin A
CAS No.:1203669-89-9
Molecular Formula:C₃₈H₆₉N₅O₁₈
Molecular Weight:883.989
Hs Code.:

Synonyms:1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-amino-6''-deoxy-kanamycin A

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Chemical Property of 1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-amino-6''-deoxy-kanamycin A

Chemical Property:

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Technology Process of 1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-amino-6''-deoxy-kanamycin A

There total 6 articles about 1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-amino-6''-deoxy-kanamycin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 953395-50-1
1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-azido-6''-deoxy-kanamycin A

: 1203669-89-9
1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-amino-6''-deoxy-kanamycin A

Guidance literature:: With 10% palladium hydroxide on charcoal; hydrogen; In methanol; for 4h;

Reference yield:

: C₄₅H₇₄N₄O₂₁S

: 1203669-89-9
1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-amino-6''-deoxy-kanamycin A

Guidance literature:: C₄₅H₇₄N₄O₂₁S; With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere;

With palladium 10% on activated carbon; hydrogen; In methanol; acetic acid; at 20 ℃; for 12h;
DOI:10.1016/j.ejmech.2019.111639

Reference yield:

: 80860-34-0
di-tert-butyl ((1S,3R,4S,5R,6R)-4-(((2S,3R,4S,5S,6R)-4-((tert-butoxycarbonyl)amino)-3,5-dihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)oxy)-6-(((2R,3R,4S,5S,6R)-6-(((tert-butoxycarbonyl)amino)methyl)-3,4,5-trihydroxytetrahydro-2H-pyran-2-yl)oxy)-5-hydroxycyclohexane-1,3-diyl)dicarbamate

: 1203669-89-9
1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-amino-6''-deoxy-kanamycin A

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 48 h

2: sodium azide / N,N-dimethyl-formamide / 60 °C

3: 10% palladium hydroxide on charcoal; hydrogen / methanol / 4 h

With pyridine; sodium azide; 10% palladium hydroxide on charcoal; hydrogen; In methanol; N,N-dimethyl-formamide;