2,6-dioxa-14,18-diazatricyclo[18.4.0.0^7,12]-tetracosa-7,9,11,20,22,24⁽¹⁾-hexaene

Base Information

• Chemical Name: 2,6-dioxa-14,18-diazatricyclo[18.4.0.0^7,12]-tetracosa-7,9,11,20,22,24⁽¹⁾-hexaene
• CAS No.: 65639-49-8
• Molecular Formula: C₂₀H₂₆N₂O₂
• Molecular Weight: 326.439

Synonyms:2,6-dioxa-14,18-diazatricyclo[18.4.0.0^7,12]-tetracosa-7,9,11,20,22,24⁽¹⁾-hexaene

Chemical Property of 2,6-dioxa-14,18-diazatricyclo[18.4.0.0^7,12]-tetracosa-7,9,11,20,22,24⁽¹⁾-hexaene

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Technology Process of 2,6-dioxa-14,18-diazatricyclo[18.4.0.0^7,12]-tetracosa-7,9,11,20,22,24⁽¹⁾-hexaene

There total 1 articles about 2,6-dioxa-14,18-diazatricyclo[18.4.0.0^7,12]-tetracosa-7,9,11,20,22,24⁽¹⁾-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Ni(OtnNtnH4)Cl2 (66793-45-1) → 2,6-dioxa-14,18-diazatricyclo[18.4.0.07,12]-tetracosa-7,9,11,20,22,24(1)-hexaene (65639-49-8) + nickel dichloride (83864-14-6)

Guidance literature:

With HCl; In water; water-d2; in 90 % D2O; Kinetics;

DOI:10.1021/ic50205a028

Reference yield: 75.0%

2,6-dioxa-14,18-diazatricyclo[18.4.0.07,12]-tetracosa-7,9,11,20,22,24(1)-hexaene (65639-49-8) + salicylaldehyde (90-02-8) → C27H30N2O3

Guidance literature:

In methanol; at 20 ℃; for 0.166667h;

DOI:10.1071/CH15204_CO

Reference yield: 43.0%

2,6-dioxa-14,18-diazatricyclo[18.4.0.07,12]-tetracosa-7,9,11,20,22,24(1)-hexaene (65639-49-8) + benzyl bromide (100-39-0) → 14,18-dibenzyl-2,6-dioxa-14,18-diaza-tricyclo[18.4.0.07,12]tetracosa-1(24),7,9,11,20,22-hexaene

Guidance literature:

With sodium carbonate; In acetonitrile; Heating;

DOI:10.1071/CH99098

upstream raw materials:

Ni(OtnNtnH₄)Cl₂

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