[3-Chloro-4-(6-chloro-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine

Base Information

• Chemical Name: [3-Chloro-4-(6-chloro-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine
• CAS No.: 113628-55-0
• Molecular Formula: C₁₇H₁₃Cl₂N₅
• Molecular Weight: 358.23

Synonyms:[3-Chloro-4-(6-chloro-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine

Chemical Property of [3-Chloro-4-(6-chloro-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of [3-Chloro-4-(6-chloro-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine

There total 3 articles about [3-Chloro-4-(6-chloro-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

{3-Chloro-4-[(4-chloro-phthalazin-1-yl)-hydrazonomethyl]-phenyl}-dimethyl-amine (87539-66-0) → [3-Chloro-4-(6-chloro-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine (113628-55-0)

Guidance literature:

With lead(IV) acetate; In acetic acid; for 1h; Ambient temperature;

DOI:10.1021/jm00401a010

Reference yield:

2-chloro-4-(dimethylamino)benzaldehyde (1424-66-4) → [3-Chloro-4-(6-chloro-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine (113628-55-0)

Guidance literature:

Multi-step reaction with 2 steps

2: lead tetracetate

With lead(IV) acetate;

Reference yield:

(3-Chloro-4-{[4-chloro-2H-phthalazin-(1Z)-ylidene]-hydrazonomethyl}-phenyl)-dimethyl-amine (87539-66-0) → [3-Chloro-4-(6-chloro-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine (113628-55-0)

Guidance literature:

With lead(IV) acetate; Yield given;

upstream raw materials:

{3-Chloro-4-[(4-chloro-phthalazin-1-yl)-hydrazonomethyl]-phenyl}-dimethyl-amine

(3-Chloro-4-{[4-chloro-2H-phthalazin-(1Z)-ylidene]-hydrazonomethyl}-phenyl)-dimethyl-amine

2-chloro-4-(dimethylamino)benzaldehyde

Downstream raw materials:

[3-Chloro-4-(6-ethoxy-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine

[3-Chloro-4-(6-pyrrolidin-1-yl-[1,2,4]triazolo[3,4-a]phthalazin-3-yl)-phenyl]-dimethyl-amine

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