Bis(1,1-dimethylethyl)-(2-iodo-4-nitrophenyl) imidodicarbonate

Base Information

Chemical Name:Bis(1,1-dimethylethyl)-(2-iodo-4-nitrophenyl) imidodicarbonate
CAS No.:395639-04-0
Molecular Formula:C₁₆H₂₁IN₂O₆
Molecular Weight:464.257
Hs Code.:
DSSTox Substance ID:DTXSID401163053
Nikkaji Number:J1.604.036C

Synonyms:395639-04-0;Bis(1,1-dimethylethyl)-(2-iodo-4-nitrophenyl) imidodicarbonate;Imidodicarbonic acid, 2-(2-iodo-4-nitrophenyl)-, 1,3-bis(1,1-dimethylethyl) ester;tert-butyl N-(2-iodo-4-nitrophenyl)-N-[(2-methylpropan-2-yl)oxycarbonyl]carbamate;DTXSID401163053;MFCD14635642;AKOS037644094;AS-44485;Bis(1,1-dimethylethyl)-(2-iodo-4-nitrophenyl)imidodicarbonate;1,3-Bis(1,1-dimethylethyl) 2-(2-iodo-4-nitrophenyl)imidodicarbonate

Suppliers and Price of Bis(1,1-dimethylethyl)-(2-iodo-4-nitrophenyl) imidodicarbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bis(1,1-dimethylethyl)-(2-iodo-4-nitrophenyl) imidodicarbonate

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:464.04443
Heavy Atom Count:25
Complexity:492

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)OC(=O)N(C1=C(C=C(C=C1)[N+](=O)[O-])I)C(=O)OC(C)(C)C

Technology Process of Bis(1,1-dimethylethyl)-(2-iodo-4-nitrophenyl) imidodicarbonate

There total 1 articles about Bis(1,1-dimethylethyl)-(2-iodo-4-nitrophenyl) imidodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 6293-83-0
2-iodo-4-nitrophenylamine

: 395639-04-0
bis(1,1-dimethylethyl)(2-iodo-4-nitrophenyl)imidocarbonate

Guidance literature:: With dmap; In tetrahydrofuran; for 31h; Ambient temperature;
DOI:10.1016/0040-4020(95)00601-4

Reference yield: 94.0%

: 395639-04-0
bis(1,1-dimethylethyl)(2-iodo-4-nitrophenyl)imidocarbonate

: 171513-06-7
1,1-dimethylethyl (2-iodo-4-nitrophenyl)carbamate

Guidance literature:: With nitric acid; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1016/S0040-4020(01)00900-0

Reference yield: 61.0%

: 106-95-6
allyl bromide

: 395639-04-0
bis(1,1-dimethylethyl)(2-iodo-4-nitrophenyl)imidocarbonate

: di(tert-butyl) 2-allyl-4-nitrophenylimidodicarbonate

Guidance literature:: bis(1,1-dimethylethyl)(2-iodo-4-nitrophenyl)imidocarbonate; With phenylmagnesium chloride; In tetrahydrofuran; at -78 ℃; for 0.5h;

In tetrahydrofuran;

allyl bromide; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/jo048132o