tert-butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-phenoxypropoxy}dimethylsilane 3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichlorobenzyloxy)phenyl]propan-1-ol

Base Information

Chemical Name:tert-butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-phenoxypropoxy}dimethylsilane 3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichlorobenzyloxy)phenyl]propan-1-ol
CAS No.:1202577-20-5
Molecular Formula:C₂₈H₃₄Cl₂O₃Si
Molecular Weight:517.568
Hs Code.:

tert-butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-phenoxypropoxy}dimethylsilane 3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichlorobenzyloxy)phenyl]propan-1-ol

Synonyms:tert-butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-phenoxypropoxy}dimethylsilane 3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichlorobenzyloxy)phenyl]propan-1-ol

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Chemical Property of tert-butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-phenoxypropoxy}dimethylsilane 3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichlorobenzyloxy)phenyl]propan-1-ol

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Technology Process of tert-butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-phenoxypropoxy}dimethylsilane 3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichlorobenzyloxy)phenyl]propan-1-ol

There total 4 articles about tert-butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-phenoxypropoxy}dimethylsilane 3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichlorobenzyloxy)phenyl]propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1202577-14-7
3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichloro benzyloxy)phenyl]propan-1-ol

: 108-95-2,27073-41-2
phenol

: 1202577-20-5
tert-butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-phenoxypropoxy}dimethylsilane 3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichlorobenzyloxy)phenyl]propan-1-ol

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 20 ℃; for 5h; Inert atmosphere;

Reference yield:

: 106-41-2
4-bromo-phenol

: 1202577-20-5
tert-butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-phenoxypropoxy}dimethylsilane 3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichlorobenzyloxy)phenyl]propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 20 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere

2.2: 0.08 h / -78 °C

3.1: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

With n-butyllithium; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; toluene;

Reference yield:

: 1805-32-9
3,4-dichlorobenzyl alcohol

: 1202577-20-5
tert-butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-phenoxypropoxy}dimethylsilane 3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichlorobenzyloxy)phenyl]propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 20 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere

2.2: 0.08 h / -78 °C

3.1: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

With n-butyllithium; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; toluene;