Technology Process of C17H14FNO6
There total 3 articles about C17H14FNO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H18FNO6;
With
2,4,6-trimethyl-pyridine; lithium iodide;
at 180 ℃;
for 2h;
Inert atmosphere;
With
hydrogenchloride;
In
water;
at 20 ℃;
for 0.5h;
Inert atmosphere;
Cooling with ice;
DOI:10.1002/cmdc.201200334
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: thionyl chloride; N,N-dimethyl-formamide / 2 h / Inert atmosphere; Reflux
1.2: Schotten-Baumann Reaction / 24 h / Inert atmosphere; Reflux
1.3: Inert atmosphere
2.1: lithium iodide; 2,4,6-trimethyl-pyridine / neat (no solvent) / 2 h / 180 °C / Inert atmosphere
2.2: 0.5 h / 20 °C / Inert atmosphere; Cooling with ice
With
2,4,6-trimethyl-pyridine; thionyl chloride; N,N-dimethyl-formamide; lithium iodide;
In
neat (no solvent);
DOI:10.1002/cmdc.201200334
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: thionyl chloride; N,N-dimethyl-formamide / 2 h / Inert atmosphere; Reflux
1.2: Schotten-Baumann Reaction / 24 h / Inert atmosphere; Reflux
1.3: Inert atmosphere
2.1: lithium iodide; 2,4,6-trimethyl-pyridine / neat (no solvent) / 2 h / 180 °C / Inert atmosphere
2.2: 0.5 h / 20 °C / Inert atmosphere; Cooling with ice
With
2,4,6-trimethyl-pyridine; thionyl chloride; N,N-dimethyl-formamide; lithium iodide;
In
neat (no solvent);
DOI:10.1002/cmdc.201200334
