ethyl [(2-acetoxy-3-methoxyphenyl)hydroxymethylidene]ethoxycarbonylacetate

Base Information

Chemical Name:ethyl [(2-acetoxy-3-methoxyphenyl)hydroxymethylidene]ethoxycarbonylacetate
CAS No.:367526-60-1
Molecular Formula:C₁₇H₂₀O₈
Molecular Weight:352.341
Hs Code.:

Synonyms:ethyl [(2-acetoxy-3-methoxyphenyl)hydroxymethylidene]ethoxycarbonylacetate

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Chemical Property of ethyl [(2-acetoxy-3-methoxyphenyl)hydroxymethylidene]ethoxycarbonylacetate

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Technology Process of ethyl [(2-acetoxy-3-methoxyphenyl)hydroxymethylidene]ethoxycarbonylacetate

There total 4 articles about ethyl [(2-acetoxy-3-methoxyphenyl)hydroxymethylidene]ethoxycarbonylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2554-82-7
2-acetoxy-3-methoxybenzoic acid

: 367526-60-1
ethyl [(2-acetoxy-3-methoxyphenyl)hydroxymethylidene]ethoxycarbonylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: DCC / tetrahydrofuran / 3 - 5 °C

2: 2.0 g / NaH / tetrahydrofuran / 2.5 h / 20 °C

With sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1055/s-2004-829132

Reference yield:

: 105-53-3
diethyl malonate

: 2-acetoxy-3-methoxy-benzoic acid benzotriazol-1-yl ester

: 367526-60-1
ethyl [(2-acetoxy-3-methoxyphenyl)hydroxymethylidene]ethoxycarbonylacetate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 2.5h;
DOI:10.1055/s-2004-829132

Reference yield:

: 58778-45-3
2-(chlorocarbonyl)-6-methoxyphenyl acetate

: 105-53-3
diethyl malonate

: 367526-60-1
ethyl [(2-acetoxy-3-methoxyphenyl)hydroxymethylidene]ethoxycarbonylacetate

Guidance literature:: diethyl malonate; With ethanol; magnesium; In tetrachloromethane; toluene; for 1h; Heating;

2-(chlorocarbonyl)-6-methoxyphenyl acetate; In tetrachloromethane; toluene; at 20 ℃; for 0.5h;
DOI:10.1081/SCC-100104333