1-Decanesulfonyl fluoride

Base Information

• Chemical Name: 1-Decanesulfonyl fluoride
• CAS No.: 68259-13-2
• Molecular Formula: C10H21FO2S
• Molecular Weight: 224.3359
• DSSTox Substance ID: DTXSID3071357
• Nikkaji Number: J429.785G
• Wikidata: Q81998965
• Mol file: 68259-13-2.mol

Synonyms:1-Decanesulfonyl fluoride;decane-1-sulfonyl fluoride;68259-13-2;1-Decanesulfonic acid fluoride;C10H21FO2S;SCHEMBL1469647;DTXSID3071357;C10-H21-F-O2-S;EN300-1451136

Chemical Property of 1-Decanesulfonyl fluoride

Chemical Property:

• Vapor Pressure: 0.00299mmHg at 25°C
• Boiling Point: 293.6°Cat760mmHg
• Flash Point: 131.4°C
• PSA: 42.52000
• Density: 1.019g/cm³
• LogP: 4.50720
• XLogP3: 4.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 9
• Exact Mass: 224.12462924
• Heavy Atom Count: 14
• Complexity: 207

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCS(=O)(=O)F

Technology Process of 1-Decanesulfonyl fluoride

There total 4 articles about 1-Decanesulfonyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

didecyl disulfide (10496-18-1) → decylsulfonylfluoride (68259-13-2)

Guidance literature:

With water; Selectfluor; In acetonitrile; for 1h; Reflux;

DOI:10.1016/j.tetlet.2011.03.132

Reference yield: 91.0%

di-n-decyl thiosulfonate (1309877-85-7) → decylsulfonylfluoride (68259-13-2)

Guidance literature:

With Selectfluor; In water; acetonitrile; at 20 ℃; for 1h; Reflux;

DOI:10.1016/j.tet.2014.02.013

Reference yield: 90.0%

1-Iodooctane (629-27-6) + ethylenesulfonyl fluoride (677-25-8) → decylsulfonylfluoride (68259-13-2)

Guidance literature:

With dimanganese decacarbonyl; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; In dimethyl sulfoxide; at 20 ℃; for 24h; Inert atmosphere; Irradiation;

DOI:10.1002/adsc.202000515

upstream raw materials:

didecyl disulfide

di-n-decyl thiosulfonate

1-Iodooctane

ethylenesulfonyl fluoride