di-n-decyl thiosulfonate

Base Information

• Chemical Name: di-n-decyl thiosulfonate
• CAS No.: 1309877-85-7
• Molecular Formula: C₂₀H₄₂O₂S₂
• Molecular Weight: 378.684

Synonyms:di-n-decyl thiosulfonate

Chemical Property of di-n-decyl thiosulfonate

Chemical Property:

Purity/Quality:

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Technology Process of di-n-decyl thiosulfonate

There total 1 articles about di-n-decyl thiosulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

didecyl disulfide (10496-18-1) → decylsulfonylfluoride (68259-13-2) + di-n-decyl thiosulfonate (1309877-85-7)

Guidance literature:

With water; Selectfluor; In acetonitrile; at 20 ℃; for 0.333333h;

DOI:10.1016/j.tetlet.2011.03.132

Reference yield: 91.0%

di-n-decyl thiosulfonate (1309877-85-7) → decylsulfonylfluoride (68259-13-2)

Guidance literature:

With Selectfluor; In water; acetonitrile; at 20 ℃; for 1h; Reflux;

DOI:10.1016/j.tet.2014.02.013

Reference yield: 76.0%

di-n-decyl thiosulfonate (1309877-85-7) + trimethyl(pentafluorophenyl)silane (1206-46-8) → 1-{(2,3,4,5,6-pentafluorophenyl)thio}decane

Guidance literature:

With phosphazene base-P₄-tert-butyl; In tetrahydrofuran; at 20 ℃; for 20h; Inert atmosphere; Schlenk technique; Molecular sieve; Green chemistry;

DOI:10.1039/d1ob01350e

upstream raw materials:

didecyl disulfide

Downstream raw materials:

decylsulfonylfluoride

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