4-Diethylaminomethyl-cyclohexanecarboxylic acid 2-sulfamoyl-benzothiazol-6-yl ester

Base Information

Chemical Name:4-Diethylaminomethyl-cyclohexanecarboxylic acid 2-sulfamoyl-benzothiazol-6-yl ester
CAS No.:121811-00-5
Molecular Formula:C₁₉H₂₇N₃O₄S₂
Molecular Weight:425.573
Hs Code.:

Synonyms:4-Diethylaminomethyl-cyclohexanecarboxylic acid 2-sulfamoyl-benzothiazol-6-yl ester

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Chemical Property of 4-Diethylaminomethyl-cyclohexanecarboxylic acid 2-sulfamoyl-benzothiazol-6-yl ester

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Technology Process of 4-Diethylaminomethyl-cyclohexanecarboxylic acid 2-sulfamoyl-benzothiazol-6-yl ester

There total 3 articles about 4-Diethylaminomethyl-cyclohexanecarboxylic acid 2-sulfamoyl-benzothiazol-6-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 452-35-7
6-ethoxybenzothiazole-2-sulfonamide

: 121811-00-5
4-Diethylaminomethyl-cyclohexanecarboxylic acid 2-sulfamoyl-benzothiazol-6-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / AlCl₃ / 1,2-dichloro-ethane / 20 h / 25 °C

2: 19 percent / pyridine, 4-(dimethylamino)pyridine / 1.5 h / 25 °C

With pyridine; dmap; aluminium trichloride; In 1,2-dichloro-ethane;
DOI:10.1021/jm00131a011

Reference yield:

: 120-53-6
6-ethoxy-2-mercaptobenzothiazole

: 121811-00-5
4-Diethylaminomethyl-cyclohexanecarboxylic acid 2-sulfamoyl-benzothiazol-6-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: conc. NH₄OH, NaOCl, 2.01 M aq. NaOH / 0.25 h / 0 - 5 °C

2: 80 percent / KMnO₄, 1 N H₂SO₄ / acetone; H₂O / 1 h / pH=8.0 - 8.1

3: 66 percent / AlCl₃ / 1,2-dichloro-ethane / 20 h / 25 °C

4: 19 percent / pyridine, 4-(dimethylamino)pyridine / 1.5 h / 25 °C

With pyridine; dmap; ammonium hydroxide; sodium hydroxide; sodium hypochlorite; potassium permanganate; sulfuric acid; aluminium trichloride; In water; 1,2-dichloro-ethane; acetone;
DOI:10.1021/jm00131a011

Reference yield:

: 5304-15-4
6-ethoxy-2-benzothiazolesulfenamide

: 121811-00-5
4-Diethylaminomethyl-cyclohexanecarboxylic acid 2-sulfamoyl-benzothiazol-6-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / KMnO₄, 1 N H₂SO₄ / acetone; H₂O / 1 h / pH=8.0 - 8.1

2: 66 percent / AlCl₃ / 1,2-dichloro-ethane / 20 h / 25 °C

3: 19 percent / pyridine, 4-(dimethylamino)pyridine / 1.5 h / 25 °C

With pyridine; dmap; potassium permanganate; sulfuric acid; aluminium trichloride; In water; 1,2-dichloro-ethane; acetone;
DOI:10.1021/jm00131a011