isopropyl 2-(2-hydroxy-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate

Base Information

• Chemical Name: isopropyl 2-(2-hydroxy-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate
• CAS No.: 1266105-32-1
• Molecular Formula: C₂₁H₃₁NO₇S
• Molecular Weight: 441.546

Synonyms:isopropyl 2-(2-hydroxy-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate

Chemical Property of isopropyl 2-(2-hydroxy-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate

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Technology Process of isopropyl 2-(2-hydroxy-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate

There total 1 articles about isopropyl 2-(2-hydroxy-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

2-iodo-propane (75-30-9) + (4,5)-2-(2-hydroxy-3-{2-[2-(2-methoxyethoxy)ethoxy]-ethoxy}phenyl)-4-methyl-4,5-dihydrothiazole-1,3-thiazole-4-carboxylic acid (945635-15-4) → isopropyl 2-(2-hydroxy-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate (1266105-32-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 168h; Inert atmosphere;

Reference yield: 85.0%

1-pyrrolidinecarbonyl chloride (1192-63-8) + isopropyl 2-(2-hydroxy-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate (1266105-32-1) → isopropyl 2-(3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-2-(pyrrolidine-1-carbonyloxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate (1266105-33-2)

Guidance literature:

With pyridine; dmap; triethylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

Reference yield: 73.0%

isopropyl 2-(2-hydroxy-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate (1266105-32-1) + N-phenyl-N-methylcarbamoyl chloride (4285-42-1) → isopropyl 2-(3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-2-((methyl)(phenyl)carbamoyloxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate (1266105-35-4)

Guidance literature:

With dmap; triethylamine; In pyridine; dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

upstream raw materials:

2-iodo-propane

(4,5)-2-(2-hydroxy-3-{2-[2-(2-methoxyethoxy)ethoxy]-ethoxy}phenyl)-4-methyl-4,5-dihydrothiazole-1,3-thiazole-4-carboxylic acid

Downstream raw materials:

isopropyl 2-(3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-2-((methyl)(phenyl)carbamoyloxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate

isopropyl 2-(3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-2-(pyrrolidine-1-carbonyloxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylate

2-(3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-2-((methyl)(phenyl)carbamoyloxy)phenyl)-4(S)-methyl-4,5-dihydrothiazole-4-carboxylic acid

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