N^δ-(allyloxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol

Base Information

Chemical Name:N^δ-(allyloxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol
CAS No.:854443-22-4
Molecular Formula:C₃₀H₄₃N₃O₄Si
Molecular Weight:537.775
Hs Code.:

N<sup>δ</sup>-(allyloxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol

Synonyms:N^δ-(allyloxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol

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Chemical Property of N^δ-(allyloxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol

Chemical Property:

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Technology Process of N^δ-(allyloxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol

There total 4 articles about N^δ-(allyloxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 854443-30-4
N^δ-(allyloxycarbonyl)-N^α-(fluoren-9-ylmethoxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol

: 854443-22-4
N^δ-(allyloxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol

Guidance literature:: With morpholine; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2005.03.061

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 854443-22-4
N^δ-(allyloxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / imidazole / CH₂Cl₂ / 3 h / 20 °C

2: 82 percent / O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium PF₆; diisopropylethylamine / dimethylformamide / 3 h / 0 - 20 °C

3: 94 percent / morpholine / 2 h / 20 °C

With morpholine; 1H-imidazole; N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.03.061

Reference yield:

: 209627-36-1
(2S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)idinepyrrol

: 854443-22-4
N^δ-(allyloxycarbonyl)-L-ornithyl-O-(tert-butyldiphenylsilyl)-L-prolinol

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium PF₆; diisopropylethylamine / dimethylformamide / 3 h / 0 - 20 °C

2: 94 percent / morpholine / 2 h / 20 °C

With morpholine; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.03.061