Technology Process of 2,6-Dibenzofurandicarboxylic acid, 3,9-dimethoxy-1,7-dimethyl-,
2-methyl 6-(phenylmethyl) ester
There total 21 articles about 2,6-Dibenzofurandicarboxylic acid, 3,9-dimethoxy-1,7-dimethyl-,
2-methyl 6-(phenylmethyl) ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 87 percent / potassium carbonate / dimethylsulfoxide / 2 h / Ambient temperature
2: 97 percent / H2 / 10percent Pd/C / ethyl acetate / 2 h
3: 60 percent / ethyl acetate / 0.08 h / Ambient temperature
4: 90 percent / potassium carbonate / acetone / 27 h / Heating
5: 58 percent / palladium acetate, trifluoroacetic acid / acetic acid / 4.5 h / Ambient temperature
With
hydrogen; palladium diacetate; potassium carbonate; trifluoroacetic acid;
palladium on activated charcoal;
In
acetic acid; dimethyl sulfoxide; ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 97 percent / H2 / 10percent Pd/C / ethyl acetate / 2 h
2: 60 percent / ethyl acetate / 0.08 h / Ambient temperature
3: 90 percent / potassium carbonate / acetone / 27 h / Heating
4: 58 percent / palladium acetate, trifluoroacetic acid / acetic acid / 4.5 h / Ambient temperature
With
hydrogen; palladium diacetate; potassium carbonate; trifluoroacetic acid;
palladium on activated charcoal;
In
acetic acid; ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 11 steps
1: 12.7 g / tetrahydrofuran / 120 h / Ambient temperature
2: 13.0 g / sodium acetate / 0.33 h / Heating
3: 8.5 g / LiAlH4 / tetrahydrofuran / 0.5 h / Heating
4: 6.8 g / H2, conc. HCl / Pd/C / methanol / 48 h
5: 3.2 g / phosphoryl chloride / 3 h / Ambient temperature
6: 3.0 g / potassium carbonate / dimethylformamide / 3 h / Ambient temperature
7: 3.0 g / potassium permanganate, pyridine / H2O / 0.33 h / 85 °C
8: potassium carbonate / dimethylformamide / Ambient temperature
9: 48 mg / titanium tetrachloride / CH2Cl2 / 1 h / -10 °C
10: potassium permanganate, pyridine / H2O / 0.33 h / 85 °C
11: 105 mg / potassium carbonate / dimethylformamide / Ambient temperature
With
pyridine; hydrogenchloride; potassium permanganate; lithium aluminium tetrahydride; hydrogen; sodium acetate; titanium tetrachloride; potassium carbonate; trichlorophosphate;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
