(Z)-2-((4-methylbenzenesulfonamido)(methylsulfanyl)-methyleneamino)benzoic acid

Base Information

Chemical Name:(Z)-2-((4-methylbenzenesulfonamido)(methylsulfanyl)-methyleneamino)benzoic acid
CAS No.:1452849-70-5
Molecular Formula:C₁₆H₁₆N₂O₄S₂
Molecular Weight:364.446
Hs Code.:

Synonyms:(Z)-2-((4-methylbenzenesulfonamido)(methylsulfanyl)-methyleneamino)benzoic acid

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Chemical Property of (Z)-2-((4-methylbenzenesulfonamido)(methylsulfanyl)-methyleneamino)benzoic acid

Chemical Property:

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Technology Process of (Z)-2-((4-methylbenzenesulfonamido)(methylsulfanyl)-methyleneamino)benzoic acid

There total 7 articles about (Z)-2-((4-methylbenzenesulfonamido)(methylsulfanyl)-methyleneamino)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1452849-69-2
(Z)-tert-butyl 2-((4-methylbenzenesulfonamido)(methylsulfanyl)-methyleneamino)benzoate

: 1452849-70-5
(Z)-2-((4-methylbenzenesulfonamido)(methylsulfanyl)-methyleneamino)benzoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jo4010876

Reference yield:

: 55666-41-6
tert-butyl 2-nitrobenzoate

: 1452849-70-5
(Z)-2-((4-methylbenzenesulfonamido)(methylsulfanyl)-methyleneamino)benzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium on activated charcoal; hydrogen / ethanol / 72 h / 1520.1 Torr

2.1: triethylamine / ethyl acetate / 0.5 h / -78 °C

2.2: 20.5 h / -78 - 20 °C

3.1: potassium carbonate / acetone / 20 h / Reflux

4.1: water; sodium hydroxide / ethanol / 2 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

With palladium on activated charcoal; water; hydrogen; potassium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; ethyl acetate; acetone;
DOI:10.1021/jo4010876

Reference yield:

: 890091-28-8
tert-butyl 2-isothiocyanatobenzoate

: 1452849-70-5
(Z)-2-((4-methylbenzenesulfonamido)(methylsulfanyl)-methyleneamino)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 20 h / Reflux

2: water; sodium hydroxide / ethanol / 2 h / 20 °C

3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

With water; potassium carbonate; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; acetone;
DOI:10.1021/jo4010876