C₄₆H₅₈N₄O₆

Base Information

• Chemical Name: C₄₆H₅₈N₄O₆
• CAS No.: 144582-40-1
• Molecular Formula: C₄₆H₅₈N₄O₆
• Molecular Weight: 762.99
• Mol file: 144582-40-1.mol

Synonyms:C₄₆H₅₈N₄O₆

Chemical Property of C₄₆H₅₈N₄O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₆H₅₈N₄O₆

There total 18 articles about C₄₆H₅₈N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-bis-(3-bromopropyl)-benzene (19417-59-5) → C46H58N4O6 (144582-40-1)

Guidance literature:

Multi-step reaction with 13 steps

1: 1) NaOEt, 2) aq. KOH / 1) EtOH

2: dimethylformamide / Heating

3: SOCl₂ / Heating

4: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

5: B₂H₆ / tetrahydrofuran

6: PhCH₂ONa / Heating

7: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

8: dimethylformamide / Heating

9: POCl₃ / CH₂Cl₂

10: cyclohexylamine / toluene / Heating

11: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

12: acetic acid / 70 °C

13: aq. KOH / propan-1-ol / Heating

With potassium hydroxide; thionyl chloride; sulfuryl dichloride; hydrogen; sodium ethanolate; tin(IV) chloride; cyclohexylamine; sodium phenyl-methanolate; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; propan-1-ol; nitromethane; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene;

Reference yield:

[1,4-phenylene]-bis(3-hydroxypropane) (19417-58-4) → C46H58N4O6 (144582-40-1)

Guidance literature:

Multi-step reaction with 14 steps

1: HBr

2: 1) NaOEt, 2) aq. KOH / 1) EtOH

3: dimethylformamide / Heating

4: SOCl₂ / Heating

5: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

6: B₂H₆ / tetrahydrofuran

7: PhCH₂ONa / Heating

8: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

9: dimethylformamide / Heating

10: POCl₃ / CH₂Cl₂

11: cyclohexylamine / toluene / Heating

12: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

13: acetic acid / 70 °C

14: aq. KOH / propan-1-ol / Heating

With potassium hydroxide; thionyl chloride; sulfuryl dichloride; hydrogen bromide; hydrogen; sodium ethanolate; tin(IV) chloride; cyclohexylamine; sodium phenyl-methanolate; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; propan-1-ol; nitromethane; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene;

Reference yield:

3,3'-(1,4-phenylene)dipropanoic acid (4251-21-2) → C46H58N4O6 (144582-40-1)

Guidance literature:

Multi-step reaction with 16 steps

1: 1) SOCl₂, 2) NEt₃

2: B₂H₆

3: HBr

4: 1) NaOEt, 2) aq. KOH / 1) EtOH

5: dimethylformamide / Heating

6: SOCl₂ / Heating

7: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

8: B₂H₆ / tetrahydrofuran

9: PhCH₂ONa / Heating

10: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

11: dimethylformamide / Heating

12: POCl₃ / CH₂Cl₂

13: cyclohexylamine / toluene / Heating

14: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

15: acetic acid / 70 °C

16: aq. KOH / propan-1-ol / Heating

With potassium hydroxide; thionyl chloride; sulfuryl dichloride; hydrogen bromide; hydrogen; sodium ethanolate; tin(IV) chloride; cyclohexylamine; triethylamine; sodium phenyl-methanolate; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; propan-1-ol; nitromethane; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene;

upstream raw materials:

C₅₈H₇₂N₆O₈

[1,4-phenylene]-bis(3-hydroxypropane)

1,4-bis-(3-bromopropyl)-benzene

3,3'-(1,4-phenylene)dipropanoic acid