C₂₃H₃₈N₂O₂Si

Base Information

Chemical Name:C₂₃H₃₈N₂O₂Si
CAS No.:1255097-45-0
Molecular Formula:C₂₃H₃₈N₂O₂Si
Molecular Weight:402.652
Hs Code.:

C<sub>23</sub>H<sub>38</sub>N<sub>2</sub>O<sub>2</sub>Si

Synonyms:C₂₃H₃₈N₂O₂Si

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Chemical Property of C₂₃H₃₈N₂O₂Si

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Technology Process of C₂₃H₃₈N₂O₂Si

There total 6 articles about C₂₃H₃₈N₂O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1255097-44-9
C₁₀H₁₈N₂O

: 69739-34-0
t-butyldimethylsiyl triflate

: 100-52-7
benzaldehyde

: 1255097-45-0
C₂₃H₃₈N₂O₂Si

Guidance literature:: C₁₀H₁₈N₂O; With n-butyllithium; In tetrahydrofuran; at 0 ℃;

benzaldehyde; In tetrahydrofuran; at -78 - 0 ℃;

t-butyldimethylsiyl triflate; In tetrahydrofuran; at -78 - 0 ℃; optical yield given as %de;
DOI:10.1246/cl.2010.835

Reference yield:

: 562-13-0
2,2-dimethyl-1,3-cyclohexanedione

: 1255097-45-0
C₂₃H₃₈N₂O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 - 0 °C

2.1: (-)-diisopinocamphenylborane chloride / 24 h / 20 °C

3.1: N-iodo-succinimide / dichloromethane / 2 h / -40 - 20 °C

4.1: 2,6-dimethylpyridine; silver trifluoromethanesulfonate / dichloromethane / 2 h / 40 °C

5.1: acetic acid / ethanol / 12 h / 70 °C

6.1: n-butyllithium / tetrahydrofuran / 0 °C

6.2: -78 - 0 °C

6.3: -78 - 0 °C

With 2,6-dimethylpyridine; N-iodo-succinimide; n-butyllithium; silver trifluoromethanesulfonate; potassium hexamethylsilazane; acetic acid; (-)-diisopinocamphenylborane chloride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1246/cl.2010.835

Reference yield:

: 1255097-40-5
C₁₇H₃₂O₂Si

: 1255097-45-0
C₂₃H₃₈N₂O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: (-)-diisopinocamphenylborane chloride / 24 h / 20 °C

2.1: N-iodo-succinimide / dichloromethane / 2 h / -40 - 20 °C

3.1: 2,6-dimethylpyridine; silver trifluoromethanesulfonate / dichloromethane / 2 h / 40 °C

4.1: acetic acid / ethanol / 12 h / 70 °C

5.1: n-butyllithium / tetrahydrofuran / 0 °C

5.2: -78 - 0 °C

5.3: -78 - 0 °C

With 2,6-dimethylpyridine; N-iodo-succinimide; n-butyllithium; silver trifluoromethanesulfonate; acetic acid; (-)-diisopinocamphenylborane chloride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1246/cl.2010.835