2-Hydroxymethyl-4-chlor-2'-aminobenzanilid

Base Information

Chemical Name:2-Hydroxymethyl-4-chlor-2'-aminobenzanilid
CAS No.:33591-91-2
Molecular Formula:C₁₄H₁₃ClN₂O₂
Molecular Weight:276.722
Hs Code.:

Synonyms:2-Hydroxymethyl-4-chlor-2'-aminobenzanilid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Hydroxymethyl-4-chlor-2'-aminobenzanilid

Chemical Property:

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Technology Process of 2-Hydroxymethyl-4-chlor-2'-aminobenzanilid

There total 4 articles about 2-Hydroxymethyl-4-chlor-2'-aminobenzanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 59187-55-2
N-(4-chloro-2-methoxycarbonylphenyl)-(2-amino)phenylcarboxamide

: 33591-91-2
2-Hydroxymethyl-4-chlor-2'-aminobenzanilid

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 4h; Inert atmosphere;

Reference yield:

: 5202-89-1
4-chlorobenzenesulfonyl chloride

: 33591-91-2
2-Hydroxymethyl-4-chlor-2'-aminobenzanilid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

2: sodium tetrahydroborate; nickel(II) nitrate hexahydrate; methanol / 2 h / 0 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; lithium aluminium tetrahydride; nickel(II) nitrate hexahydrate; triethylamine; In tetrahydrofuran;

Reference yield:

: C₁₅H₁₁ClN₂O₅

: 33591-91-2
2-Hydroxymethyl-4-chlor-2'-aminobenzanilid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; nickel(II) nitrate hexahydrate; methanol / 2 h / 0 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; lithium aluminium tetrahydride; nickel(II) nitrate hexahydrate; In tetrahydrofuran;