(2S)-1-(t-butyldiphenylsiloxy)-14-iodo-2-(p-methoxybenzyloxy)tetradecane

Base Information

Chemical Name:(2S)-1-(t-butyldiphenylsiloxy)-14-iodo-2-(p-methoxybenzyloxy)tetradecane
CAS No.:914936-43-9
Molecular Formula:C₃₈H₅₅IO₃Si
Molecular Weight:714.843
Hs Code.:

Synonyms:(2S)-1-(t-butyldiphenylsiloxy)-14-iodo-2-(p-methoxybenzyloxy)tetradecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-1-(t-butyldiphenylsiloxy)-14-iodo-2-(p-methoxybenzyloxy)tetradecane

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Technology Process of (2S)-1-(t-butyldiphenylsiloxy)-14-iodo-2-(p-methoxybenzyloxy)tetradecane

There total 12 articles about (2S)-1-(t-butyldiphenylsiloxy)-14-iodo-2-(p-methoxybenzyloxy)tetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 914936-85-9
(13S)-14-(t-butyldiphenylsiloxy)-13-(p-methoxybenzyloxy)tetradecanol

: 914936-43-9
(2S)-1-(t-butyldiphenylsiloxy)-14-iodo-2-(p-methoxybenzyloxy)tetradecane

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In benzene; at 20 ℃; for 0.5h;
DOI:10.1021/ol062011o

Reference yield:

: 914936-41-7
(2S)-14-(t-butyldimethylsiloxy)-1-(t-butyldiphenylsiloxy)-2-(p-methoxybenzyloxy)tetradecane

: 914936-43-9
(2S)-1-(t-butyldiphenylsiloxy)-14-iodo-2-(p-methoxybenzyloxy)tetradecane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / aq. HCl / tetrahydrofuran / 6 h / 20 °C

2: 92 percent / imidazole; triphenylphosphine; iodine / benzene / 0.5 h / 20 °C

With 1H-imidazole; hydrogenchloride; iodine; triphenylphosphine; In tetrahydrofuran; benzene;
DOI:10.1021/ol062011o

Reference yield:

: 914936-39-3
(2S)-1-(t-butyldiphenylsiloxy)-4-iodo-2-(p-methoxybenzyloxy)butane

: 914936-43-9
(2S)-1-(t-butyldiphenylsiloxy)-14-iodo-2-(p-methoxybenzyloxy)tetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / cuprous(I) iodide; 2,2'-bipyridyl / tetrahydrofuran / -20 - 20 °C

2: 96 percent / aq. HCl / tetrahydrofuran / 6 h / 20 °C

3: 92 percent / imidazole; triphenylphosphine; iodine / benzene / 0.5 h / 20 °C

With 1H-imidazole; hydrogenchloride; [2,2]bipyridinyl; copper(l) iodide; iodine; triphenylphosphine; In tetrahydrofuran; benzene;
DOI:10.1021/ol062011o