2-[2-(4-Carboxymethoxy-2,3-dichloro-benzoyl)-butyl]-malonic acid diethyl ester

Base Information

Chemical Name:2-[2-(4-Carboxymethoxy-2,3-dichloro-benzoyl)-butyl]-malonic acid diethyl ester
CAS No.:183430-20-8
Molecular Formula:C₂₀H₂₄Cl₂O₈
Molecular Weight:463.312
Hs Code.:

Synonyms:2-[2-(4-Carboxymethoxy-2,3-dichloro-benzoyl)-butyl]-malonic acid diethyl ester

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Chemical Property of 2-[2-(4-Carboxymethoxy-2,3-dichloro-benzoyl)-butyl]-malonic acid diethyl ester

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Technology Process of 2-[2-(4-Carboxymethoxy-2,3-dichloro-benzoyl)-butyl]-malonic acid diethyl ester

There total 1 articles about 2-[2-(4-Carboxymethoxy-2,3-dichloro-benzoyl)-butyl]-malonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 58-54-8
ethacrynic acid

: 105-53-3
diethyl malonate

: 183430-20-8
2-[2-(4-Carboxymethoxy-2,3-dichloro-benzoyl)-butyl]-malonic acid diethyl ester

Guidance literature:: With sodium ethanolate; In ethanol; for 0.0833333h; Ambient temperature;

Reference yield: 83.0%

: 183430-20-8
2-[2-(4-Carboxymethoxy-2,3-dichloro-benzoyl)-butyl]-malonic acid diethyl ester

: 183430-21-9
4-(4-Carboxymethoxy-2,3-dichloro-benzoyl)-hexanoic acid

Guidance literature:: With hydrogenchloride; In acetic acid; for 12h; Heating;

Reference yield:

: 183430-20-8
2-[2-(4-Carboxymethoxy-2,3-dichloro-benzoyl)-butyl]-malonic acid diethyl ester

: [2,3-Dichloro-4-((2R,3S)-3-ethyl-6-oxo-tetrahydro-pyran-2-yl)-phenoxy]-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / conc. HCl / acetic acid / 12 h / Heating

2: 0.1 M NaOH, KBH₄ / H₂O / 2 h / Heating

3: acetic acid / 1 h / Heating

With hydrogenchloride; sodium hydroxide; potassium borohydride; In water; acetic acid;