3-hydroxy-5-iodo-benzamide

Base Information

Chemical Name:3-hydroxy-5-iodo-benzamide
CAS No.:269411-74-7
Molecular Formula:C₇H₆INO₂
Molecular Weight:263.035
Hs Code.:

Synonyms:3-hydroxy-5-iodo-benzamide

Suppliers and Price of 3-hydroxy-5-iodo-benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-hydroxy-5-iodo-benzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-hydroxy-5-iodo-benzamide

There total 7 articles about 3-hydroxy-5-iodo-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 269411-73-6
3-iodo-5-methoxy-benzamide

: 269411-74-7
3-hydroxy-5-iodo-benzamide

Guidance literature:: With boron tribromide; In dichloromethane; for 4h; Heating;
DOI:10.1021/jm9903242

Reference yield:

: 5327-44-6
3,5-dinitroanisole

: 269411-74-7
3-hydroxy-5-iodo-benzamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: 73 percent / sodium bicarbonate; sodium sulfide nonahydrate; methanol / 0.5 h / Heating

2.1: conc. aq. HCl; NaNO₂ / 0.25 h / 0 °C

2.2: 84 percent / KI / H₂O / Heating

3.1: 91 percent / Fe₃(CO)12; methanol / toluene / 3.5 h / Heating

4.1: 83 percent / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dimethylformamide / 2 h / 80 °C

5.1: conc. aq. HCl; NaNO₂ / 0.25 h / 0 °C

5.2: 64 percent / KI / H₂O / Heating

6.1: 78 percent / 3percent aq. H₂O₂ / 4 h / 50 °C

7.1: 82 percent / BBr₃ / CH₂Cl₂ / 4 h / Heating

With hydrogenchloride; methanol; sodium sulfide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triiron dodecarbonyl; boron tribromide; sodium hydrogencarbonate; sodium nitrite; In dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Reduction / 2.1: Diazotization / 2.2: Substitution / 3.1: Reduction / 4.1: Substitution / 5.1: Diazotization / 5.2: Substitution / 6.1: Oxidation / 7.1: Hydrolysis;
DOI:10.1021/jm9903242

Reference yield:

: 62605-98-5
1-iodo-5-methoxy-phenylamine

: 269411-74-7
3-hydroxy-5-iodo-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 83 percent / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dimethylformamide / 2 h / 80 °C

2.1: conc. aq. HCl; NaNO₂ / 0.25 h / 0 °C

2.2: 64 percent / KI / H₂O / Heating

3.1: 78 percent / 3percent aq. H₂O₂ / 4 h / 50 °C

4.1: 82 percent / BBr₃ / CH₂Cl₂ / 4 h / Heating

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; sodium nitrite; In dichloromethane; N,N-dimethyl-formamide; 1.1: Substitution / 2.1: Diazotization / 2.2: Substitution / 3.1: Oxidation / 4.1: Hydrolysis;
DOI:10.1021/jm9903242