6-(4-carbethoxyphenoxy)hexyl bromide

Base Information

• Chemical Name: 6-(4-carbethoxyphenoxy)hexyl bromide
• CAS No.: 73515-07-8
• Molecular Formula: C₁₅H₂₁BrO₃
• Molecular Weight: 329.234
• Mol file: 73515-07-8.mol

Synonyms:6-(4-carbethoxyphenoxy)hexyl bromide

Chemical Property of 6-(4-carbethoxyphenoxy)hexyl bromide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 6-(4-carbethoxyphenoxy)hexyl bromide

There total 6 articles about 6-(4-carbethoxyphenoxy)hexyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

Ethyl 4-hydroxybenzoate (120-47-8) + 1-bromo-6-hexanol (4286-55-9) → 6-(4-carbethoxyphenoxy)hexyl bromide (73515-07-8)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/ma401636e

Reference yield: 60.0%

Ethyl 4-hydroxybenzoate (120-47-8) + 1 ,6-dibromohexane (629-03-8) → 6-(4-carbethoxyphenoxy)hexyl bromide (73515-07-8)

Guidance literature:

With potassium carbonate; In acetonitrile; for 16h; Sealed tube; Reflux;

DOI:10.1039/c9cc03424b

Reference yield: 31.0%

Ethyl 4-hydroxybenzoate (120-47-8) + 1 ,6-dibromohexane (629-03-8) → 1,6-bis(4-carbethoxyphenoxy)hexane (56441-89-5) + 6-(4-carbethoxyphenoxy)hexyl bromide (73515-07-8)

Guidance literature:

With potassium carbonate; In butanone; for 16h; Heating;

DOI:10.1002/jlac.199719971116

upstream raw materials:

Ethyl 4-hydroxybenzoate

1 ,6-dibromohexane

1-bromo-6-hexanol

4-hydroxy-benzoic acid

Downstream raw materials:

4-<(6-bromohexyl)oxy>benzoic acid

diethyl [6-(4-carbethoxyphenoxy)hexyl]phosphonate

4-(6-mercaptohexyloxy)benzoic acid

4-(hex-5-yn-1-yloxy)phenyl 4-((6-bromohexyl)oxy)benzoate