6-(4-(ethoxycarbonyl)phenoxy)hexylboronic acid

Base Information

Chemical Name:6-(4-(ethoxycarbonyl)phenoxy)hexylboronic acid
CAS No.:1440956-35-3
Molecular Formula:C₁₅H₂₃BO₅
Molecular Weight:294.156
Hs Code.:

Synonyms:6-(4-(ethoxycarbonyl)phenoxy)hexylboronic acid

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Chemical Property of 6-(4-(ethoxycarbonyl)phenoxy)hexylboronic acid

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Technology Process of 6-(4-(ethoxycarbonyl)phenoxy)hexylboronic acid

There total 2 articles about 6-(4-(ethoxycarbonyl)phenoxy)hexylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1440955-95-2
ethyl 4-((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexyl)oxy)benzoate

: 1440956-35-3
6-(4-(ethoxycarbonyl)phenoxy)hexylboronic acid

Guidance literature:: ethyl 4-((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexyl)oxy)benzoate; With sodium periodate; In tetrahydrofuran; water; for 0.0833333h;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1002/anie.201206681

Reference yield:

: 73515-07-8
6-(4-carbethoxyphenoxy)hexyl bromide

: 1440956-35-3
6-(4-(ethoxycarbonyl)phenoxy)hexylboronic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide; triphenylphosphine; lithium methanolate / N,N-dimethyl-formamide / 18 h / 30 °C / Schlenk technique; Inert atmosphere

2.1: sodium periodate / water; tetrahydrofuran / 0.08 h

2.2: 20 °C

With sodium periodate; copper(l) iodide; lithium methanolate; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201206681

Reference yield: 65.0%

: 1440956-35-3
6-(4-(ethoxycarbonyl)phenoxy)hexylboronic acid

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 1440956-11-5
ethyl 4-(7,7,7-trifluoroheptyloxy)benzoate

Guidance literature:: With potassium fluoride; copper(l) iodide; silver tetrafluoroborate; 3,4,7,8-Tetramethyl-o-phenanthrolin; silver fluoride; In N,N-dimethyl-formamide; at 80 ℃; for 24h; Glovebox; Inert atmosphere;
DOI:10.1002/anie.201206681