N,N-Dimethyltetradecanamide

Base Information

• Chemical Name: N,N-Dimethyltetradecanamide
• CAS No.: 3015-65-4
• Molecular Formula: C16H33 N O
• Molecular Weight: 255.444
• Hs Code.: 2924199090
• European Community (EC) Number: 221-151-0
• NSC Number: 85836
• UNII: DV80PT7RPL
• DSSTox Substance ID: DTXSID8062787
• Nikkaji Number: J48.777E
• Wikidata: Q81990268
• Mol file: 3015-65-4.mol

Synonyms:N,N-Dimethyltetradecanamide;N,N-Dimethylmyristamide;Dimethyl myristamide;3015-65-4;Tetradecanamide, N,N-dimethyl-;EINECS 221-151-0;NSC 85836;DV80PT7RPL;BRN 1776317;NSC-85836;NSC85836;N,N-Dimethylmyristamid;UNII-DV80PT7RPL;Tetradecanamide,N-dimethyl-;NCIOpen2_005107;SCHEMBL1879225;DTXSID8062787;CHEBI:146190;WLN: 13VN1&1;AKOS005287005;LS-148882

Chemical Property of N,N-Dimethyltetradecanamide

Chemical Property:

• Vapor Pressure: 0.00064mmHg at 25°C
• Melting Point: 29 °C
• Refractive Index: 1.4545 (estimate)
• Boiling Point: 309.4°Cat760mmHg
• PKA: -0.43±0.70(Predicted)
• Flash Point: 114.3°C
• PSA: 20.31000
• Density: 0.86g/cm³
• LogP: 4.77570
• XLogP3: 5.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 12
• Exact Mass: 255.256214676
• Heavy Atom Count: 18
• Complexity: 190

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCCCCCCCCCCCCC(=O)N(C)C

Technology Process of N,N-Dimethyltetradecanamide

There total 3 articles about N,N-Dimethyltetradecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1-tridecene (2437-56-1) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → N,N-dimethyltetradecanamide (3015-65-4)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; triethylaluminum; IAd; In toluene; at 100 ℃; for 3h; regioselective reaction;

DOI:10.1246/cl.2012.298

Reference yield:

n-tetradecanoic acid (544-63-8) + dimethyl amine (124-40-3) → N,N-dimethyltetradecanamide (3015-65-4)

Guidance literature:

With ammonium hydroxide; cerium(III) nitrate hexahydrate; In water; at 210 ℃; for 3.5h; Inert atmosphere;

Reference yield:

→ N,N-dimethyltetradecanamide (3015-65-4)

Guidance literature:

/BRN= 1769950/;

upstream raw materials:

1-tridecene

N,N-dimethyl-formamide

n-tetradecanoic acid

dimethyl amine

Refernces

• 1、 Miyazaki, Yosuke,Yamada, Yuuya,Nakao, Yoshiaki,Hiyama, Tamejiro. "Regioselective hydrocarbamoylation of 1-alkenes". supporting information; experimental part. p. 298 - 300. Retrieved 2012/05/20.