C₁₄H₁₀INO₂

Base Information

Chemical Name:C₁₄H₁₀INO₂
CAS No.:1304495-16-6
Molecular Formula:C₁₄H₁₀INO₂
Molecular Weight:351.143
Hs Code.:

C<sub>14</sub>H<sub>10</sub>INO<sub>2</sub>

Synonyms:C₁₄H₁₀INO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₀INO₂

Chemical Property:

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Technology Process of C₁₄H₁₀INO₂

There total 14 articles about C₁₄H₁₀INO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 100866-04-4
[3-iodo-4-(4-methoxy-phenoxy)-phenyl]-acetonitrile

: 1304495-16-6
C₁₄H₁₀INO₂

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 15h;
DOI:10.5012/bkcs.2011.32.4.1131 DOI:10.1002/cjoc.201180382

Reference yield:

: 55912-20-4
4-chloro-3-nitrobenzyl alcohol

: 1304495-16-6
C₁₄H₁₀INO₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / water / 2 h / 20 °C

2.1: sodium iodide / acetone / 12 h / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: palladium on activated charcoal; hydrogen / ethyl acetate / 6 h / 20 °C

5.1: sulfuric acid; sodium nitrite / 0.5 h / 0 - 5 °C

5.2: 20 °C

6.1: boron tribromide / dichloromethane / 15 h / -78 - 20 °C

With hydrogenchloride; sulfuric acid; palladium on activated charcoal; hydrogen; boron tribromide; sodium hydride; sodium iodide; sodium nitrite; In dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1002/cjoc.201180382

Reference yield:

: 57403-35-7
1-chloro-4-(chloromethyl)-2-nitrobenzene

: 1304495-16-6
C₁₄H₁₀INO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium iodide / acetone / 12 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

3.1: palladium on activated charcoal; hydrogen / ethyl acetate / 6 h / 20 °C

4.1: sulfuric acid; sodium nitrite / 0.5 h / 0 - 5 °C

4.2: 20 °C

5.1: boron tribromide / dichloromethane / 15 h / -78 - 20 °C

With sulfuric acid; palladium on activated charcoal; hydrogen; boron tribromide; sodium hydride; sodium iodide; sodium nitrite; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1002/cjoc.201180382