i-Si₄Cl₁₀

Base Information

• Chemical Name: i-Si₄Cl₁₀
• CAS No.: 50683-29-9
• Molecular Formula: Cl₁₀Si₄
• Molecular Weight: 466.872
• Mol file: 50683-29-9.mol

Synonyms:i-Si₄Cl₁₀

Chemical Property of i-Si₄Cl₁₀

Chemical Property:

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Technology Process of i-Si₄Cl₁₀

There total 1 articles about i-Si₄Cl₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

perchlorotrisilane (13596-23-1) → i-Si4Cl10 (50683-29-9) + tetrakis(trichlorosilyl)silane (50350-62-4) + (Cl3Si)3SiSiCl2SiCl3 (1196525-75-3) + hexachlorodisilane (13465-77-5)

Guidance literature:

With Na(Si-t-Bu₃); In benzene; byproducts: (t-Bu3Si)4Si, t-Bu3SiSi-t-Bu3, t-Bu3SiCl; under N2 or Ar; soln. of Cl3SiSiCl2SiCl3 and Na(Si-t-Bu3) (molar ratio 1:4) in benzene stirred at ambient temp. for 1 d; detd. by (29)Si NMR spectra;

DOI:10.1021/om900763y

upstream raw materials:

perchlorotrisilane