1-(5-(Benzyloxy)-7-formylbenzo[d]thiazol-2-yl)-3-ethylurea

Base Information

Chemical Name:1-(5-(Benzyloxy)-7-formylbenzo[d]thiazol-2-yl)-3-ethylurea
CAS No.:1372548-48-5
Molecular Formula:C₁₈H₁₇N₃O₃S
Molecular Weight:355.417
Hs Code.:

Synonyms:1-(5-(Benzyloxy)-7-formylbenzo[d]thiazol-2-yl)-3-ethylurea

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Chemical Property of 1-(5-(Benzyloxy)-7-formylbenzo[d]thiazol-2-yl)-3-ethylurea

Chemical Property:

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Technology Process of 1-(5-(Benzyloxy)-7-formylbenzo[d]thiazol-2-yl)-3-ethylurea

There total 11 articles about 1-(5-(Benzyloxy)-7-formylbenzo[d]thiazol-2-yl)-3-ethylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372548-11-2
1-(5-(benzyloxy)-7-cyanobenzo[d]thiazol-2-yl)-3-ethylurea

: 1372548-48-5
1-(5-(Benzyloxy)-7-formylbenzo[d]thiazol-2-yl)-3-ethylurea

Guidance literature:: 1-(5-(benzyloxy)-7-cyanobenzo[d]thiazol-2-yl)-3-ethylurea; With formic acid; aluminum nickel alloy; In water; at 95 ℃; for 5h; Inert atmosphere;

With sodium hydroxide; In water; pH=9;

Reference yield:

: 121-88-0
5-Nitro-2-aminophenol

: 1372548-48-5
1-(5-(Benzyloxy)-7-formylbenzo[d]thiazol-2-yl)-3-ethylurea

Guidance literature:: Multi-step reaction with 10 steps

1.1: bromine / acetonitrile / 1 h / 30 - 35 °C / Industry scale

2.1: sulfuric acid; sodium nitrite / ethanol / -10 - 55 °C

3.1: potassium carbonate / acetone / 3 h / Reflux; Industry scale

4.1: tin(II) chloride dihdyrate / tetrahydrofuran / 3 h / Reflux; Industry scale

4.2: 0 - 5 °C

5.1: acetone / 0.75 h / 20 °C

6.1: water; sodium hydroxide / tetrahydrofuran / 69 - 70 °C

7.1: bromine / acetonitrile / 1.5 h / 0 - 20 °C

8.1: 1,4-dioxane / 80 - 85 °C

9.1: 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc diacetate; zinc / water; N,N-dimethyl-formamide / 18 h / 100 °C / Inert atmosphere; Sealed tube

10.1: formic acid / aluminum nickel alloy / water / 5 h / 95 °C / Inert atmosphere

10.2: pH 9

With formic acid; tin(II) chloride dihdyrate; sulfuric acid; water; bromine; potassium carbonate; sodium hydroxide; sodium nitrite; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc diacetate; zinc; In tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 116632-23-6
3-bromo-5-nitro-phenol

: 1372548-48-5
1-(5-(Benzyloxy)-7-formylbenzo[d]thiazol-2-yl)-3-ethylurea

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / acetone / 3 h / Reflux; Industry scale

2.1: tin(II) chloride dihdyrate / tetrahydrofuran / 3 h / Reflux; Industry scale

2.2: 0 - 5 °C

3.1: acetone / 0.75 h / 20 °C

4.1: water; sodium hydroxide / tetrahydrofuran / 69 - 70 °C

5.1: bromine / acetonitrile / 1.5 h / 0 - 20 °C

6.1: 1,4-dioxane / 80 - 85 °C

7.1: 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc diacetate; zinc / water; N,N-dimethyl-formamide / 18 h / 100 °C / Inert atmosphere; Sealed tube

8.1: formic acid / aluminum nickel alloy / water / 5 h / 95 °C / Inert atmosphere

8.2: pH 9

With formic acid; tin(II) chloride dihdyrate; water; bromine; potassium carbonate; sodium hydroxide; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc diacetate; zinc; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; acetone; acetonitrile;