(E)-1-(5-(benzyloxy)-7-((methoxyimino)methyl)benzo[d]thiazol-2-yl)-3-ethylurea

Base Information

Chemical Name:(E)-1-(5-(benzyloxy)-7-((methoxyimino)methyl)benzo[d]thiazol-2-yl)-3-ethylurea
CAS No.:1372548-49-6
Molecular Formula:C₁₉H₂₀N₄O₃S
Molecular Weight:384.459
Hs Code.:

Synonyms:(E)-1-(5-(benzyloxy)-7-((methoxyimino)methyl)benzo[d]thiazol-2-yl)-3-ethylurea

Suppliers and Price of (E)-1-(5-(benzyloxy)-7-((methoxyimino)methyl)benzo[d]thiazol-2-yl)-3-ethylurea

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(5-(benzyloxy)-7-((methoxyimino)methyl)benzo[d]thiazol-2-yl)-3-ethylurea

Chemical Property:

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Technology Process of (E)-1-(5-(benzyloxy)-7-((methoxyimino)methyl)benzo[d]thiazol-2-yl)-3-ethylurea

There total 12 articles about (E)-1-(5-(benzyloxy)-7-((methoxyimino)methyl)benzo[d]thiazol-2-yl)-3-ethylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372548-48-5
1-(5-(Benzyloxy)-7-formylbenzo[d]thiazol-2-yl)-3-ethylurea

: 593-56-6
N-methoxylamine hydrochloride

: 1372548-49-6
(E)-1-(5-(benzyloxy)-7-((methoxyimino)methyl)benzo[d]thiazol-2-yl)-3-ethylurea

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 105 ℃; for 18h; Inert atmosphere; Sealed tube;

Reference yield:

: 1372548-11-2
1-(5-(benzyloxy)-7-cyanobenzo[d]thiazol-2-yl)-3-ethylurea

: 1372548-49-6
(E)-1-(5-(benzyloxy)-7-((methoxyimino)methyl)benzo[d]thiazol-2-yl)-3-ethylurea

Guidance literature:: Multi-step reaction with 2 steps

1.1: formic acid / aluminum nickel alloy / water / 5 h / 95 °C / Inert atmosphere

1.2: pH 9

2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 105 °C / Inert atmosphere; Sealed tube

With formic acid; N-ethyl-N,N-diisopropylamine; aluminum nickel alloy; In water; N,N-dimethyl-formamide;

Reference yield:

: 121-88-0
5-Nitro-2-aminophenol

: 1372548-49-6
(E)-1-(5-(benzyloxy)-7-((methoxyimino)methyl)benzo[d]thiazol-2-yl)-3-ethylurea

Guidance literature:: Multi-step reaction with 11 steps

1.1: bromine / acetonitrile / 1 h / 30 - 35 °C / Industry scale

2.1: sulfuric acid; sodium nitrite / ethanol / -10 - 55 °C

3.1: potassium carbonate / acetone / 3 h / Reflux; Industry scale

4.1: tin(II) chloride dihdyrate / tetrahydrofuran / 3 h / Reflux; Industry scale

4.2: 0 - 5 °C

5.1: acetone / 0.75 h / 20 °C

6.1: water; sodium hydroxide / tetrahydrofuran / 69 - 70 °C

7.1: bromine / acetonitrile / 1.5 h / 0 - 20 °C

8.1: 1,4-dioxane / 80 - 85 °C

9.1: 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc diacetate; zinc / water; N,N-dimethyl-formamide / 18 h / 100 °C / Inert atmosphere; Sealed tube

10.1: formic acid / aluminum nickel alloy / water / 5 h / 95 °C / Inert atmosphere

10.2: pH 9

11.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 105 °C / Inert atmosphere; Sealed tube

With formic acid; tin(II) chloride dihdyrate; sulfuric acid; water; bromine; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; sodium nitrite; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc diacetate; zinc; In tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; acetone; acetonitrile;