Technology Process of C24H13Cl2F3N2O4S
There total 5 articles about C24H13Cl2F3N2O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium diacetate; caesium carbonate; copper(l) chloride;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 24h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1-methyl-pyrrolidin-2-one / 4 h / 180 °C
2: tert.-butylnitrite; copper(ll) bromide / acetonitrile / 20 h / 0 - 20 °C
3: tetraphosphorus decasulfide; ethanol / 20 °C
4: ethanol / 70 °C
5: palladium diacetate; copper(l) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / N,N-dimethyl-formamide / 24 h / 100 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tert.-butylnitrite; tetraphosphorus decasulfide; ethanol; palladium diacetate; caesium carbonate; copper(l) chloride; copper(ll) bromide;
In
1-methyl-pyrrolidin-2-one; ethanol; N,N-dimethyl-formamide; acetonitrile;
5: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ethanol / 70 °C
2: palladium diacetate; copper(l) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / N,N-dimethyl-formamide / 24 h / 100 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium diacetate; caesium carbonate; copper(l) chloride;
In
ethanol; N,N-dimethyl-formamide;
2: |Suzuki Coupling;