1-benzhydryl-3-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1,3-dimethylurea

Base Information

Chemical Name:1-benzhydryl-3-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1,3-dimethylurea
CAS No.:1187857-67-5
Molecular Formula:C₂₄H₃₂N₂O₂
Molecular Weight:380.53
Hs Code.:

Synonyms:1-benzhydryl-3-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1,3-dimethylurea

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Chemical Property of 1-benzhydryl-3-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1,3-dimethylurea

Chemical Property:

Purity/Quality:

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Technology Process of 1-benzhydryl-3-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1,3-dimethylurea

There total 1 articles about 1-benzhydryl-3-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1,3-dimethylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187857-68-6
benzhydryl(methyl)carbamic chloride

: 554453-93-9
((1r,4r)-4-((methylamino)methyl)cyclohexyl)methanol

: 1187857-67-5
1-benzhydryl-3-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1,3-dimethylurea

Guidance literature:: With triethylamine; In dichloromethane; at 80 ℃; for 2h; microwave irradiation;

Reference yield:

: 1187857-67-5
1-benzhydryl-3-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1,3-dimethylurea

: 35059-50-8
t-butyl diazoacetate

: C₃₀H₄₂N₂O₄

Guidance literature:: rhodium(II) acetate; In dichloromethane; at 20 ℃; for 96h;

Reference yield:

: 1187857-67-5
1-benzhydryl-3-(((1r,4r)-4-(hydroxymethyl)cyclohexyl)methyl)-1,3-dimethylurea

: 1187857-66-4
2-(((1r,4r)-4-((3-benzhydryl-1,3-dimethylureido)methyl)cyclohexyl)methoxy)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: rhodium(II) acetate / dichloromethane / 96 h / 20 °C

2.1: water; lithium hydroxide / 2 h / 65 °C

2.2: pH 4

With water; lithium hydroxide; rhodium(II) acetate; In dichloromethane;