5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester

Base Information

Chemical Name:5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester
CAS No.:461641-24-7
Molecular Formula:C₃₅H₃₆N₂O₅S
Molecular Weight:596.747
Hs Code.:

5-isopropyl-4-[1-(toluene-4-sulfonyl)-1<i>H</i>-indol-3-yl]-1,9,9a,10a-tetrahydro-4<i>H</i>,4b<i>H</i>-10-oxa-4a-aza-indeno[1,2-<i>a</i>]indene-2-carboxylic acid ethyl ester

Synonyms:5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester

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Chemical Property of 5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester

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Technology Process of 5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester

There total 25 articles about 5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 461640-97-1
(1S,2R)-(-)-cis-1-amino-7-isopropylindan-2-ol

: 461640-91-5
ethyl (E,E)-4-oxo-2-[(N-p-toluenesulfonylindol-3-yl)vinyl]but-2-enoate

: 5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester

: 461641-24-7
5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester

Guidance literature:: In chloroform; at 20 ℃;
DOI:10.1021/ja026464+

Reference yield: 75.0%

: 461640-89-1
C₂₉H₄₁NO₂SSn

: C₆H₇IO₃

: 461640-97-1
(1S,2R)-(-)-cis-1-amino-7-isopropylindan-2-ol

: 461641-24-7
5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester

Guidance literature:: C₆H₇IO₃; (1S,2R)-(-)-cis-1-amino-7-isopropylindan-2-ol; In N,N-dimethyl-formamide; at 20 ℃; Molecular sieve;

C₂₉H₄₁NO₂SSn; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; lithium chloride; In N,N-dimethyl-formamide; at 80 ℃; for 2h; stereoselective reaction;
DOI:10.1039/c0ob00627k

Reference yield: 72.0%

: ethyl (Z)-2-iodo-4-oxobutenoate

: 461640-97-1
(1S,2R)-(-)-cis-1-amino-7-isopropylindan-2-ol

: (E)-1-(N-p-toluenesulfonyl-3-indolyl)-2-tributylstannylethene

: 5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester

: 461641-24-7
5-isopropyl-4-[1-(toluene-4-sulfonyl)-1H-indol-3-yl]-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester

Guidance literature:: With trifuran-2-yl-phosphane; 4 A molecular sieve; lithium chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In N,N-dimethyl-formamide; at 80 ℃; for 1h;
DOI:10.1021/ol061405c