methyl 14-(2,5-dichlorophenyloxy)-3,6,9,12-tetraoxatetradecanoate

Base Information

Chemical Name:methyl 14-(2,5-dichlorophenyloxy)-3,6,9,12-tetraoxatetradecanoate
CAS No.:872410-00-9
Molecular Formula:C₁₇H₂₄Cl₂O₇
Molecular Weight:411.279
Hs Code.:

Synonyms:methyl 14-(2,5-dichlorophenyloxy)-3,6,9,12-tetraoxatetradecanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 14-(2,5-dichlorophenyloxy)-3,6,9,12-tetraoxatetradecanoate

Chemical Property:

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Technology Process of methyl 14-(2,5-dichlorophenyloxy)-3,6,9,12-tetraoxatetradecanoate

There total 4 articles about methyl 14-(2,5-dichlorophenyloxy)-3,6,9,12-tetraoxatetradecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872409-96-6
2-{2-[2-(2-{2-methoxycarbomethoxy}-ethoxy)-ethoxy]-ethoxy}yl p-toluenesulfonate

: 583-78-8
2,5-dichlorophenol

: 872410-00-9
methyl 14-(2,5-dichlorophenyloxy)-3,6,9,12-tetraoxatetradecanoate

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In acetonitrile; Heating;
DOI:10.1021/ja0535357

Reference yield:

: 77303-64-1
methyl 14-hydroxy-3,6,9,12-tetraoxatetradecanoate

: 872410-00-9
methyl 14-(2,5-dichlorophenyloxy)-3,6,9,12-tetraoxatetradecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: K₂CO₃

With pyridine; potassium carbonate;
DOI:10.1002/anie.200460762

Reference yield:

: 112-60-7
Tetraethylene glycol

: 872410-00-9
methyl 14-(2,5-dichlorophenyloxy)-3,6,9,12-tetraoxatetradecanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: Na

1.2: 10 h / 100 °C

2.1: H₂SO₄ / 10 h / Heating

3.1: pyridine / cooling

4.1: 15.0 g / K₂CO₃; (n-Bu)4NI / acetonitrile / Heating

With pyridine; sulfuric acid; sodium; tetra-(n-butyl)ammonium iodide; potassium carbonate; In acetonitrile;
DOI:10.1021/ja0535357