4-{[(1'R,2'R)-1'-hydroxy-1',3'-dihydro-1H,2'H-2,2'-biinden-2'-yl]methyl}-N,N-dimethylbenzamide

Base Information

Chemical Name:4-{[(1'R,2'R)-1'-hydroxy-1',3'-dihydro-1H,2'H-2,2'-biinden-2'-yl]methyl}-N,N-dimethylbenzamide
CAS No.:1421332-96-8
Molecular Formula:C₂₈H₂₇NO₂
Molecular Weight:409.528
Hs Code.:

Synonyms:4-{[(1'R,2'R)-1'-hydroxy-1',3'-dihydro-1H,2'H-2,2'-biinden-2'-yl]methyl}-N,N-dimethylbenzamide

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Chemical Property of 4-{[(1'R,2'R)-1'-hydroxy-1',3'-dihydro-1H,2'H-2,2'-biinden-2'-yl]methyl}-N,N-dimethylbenzamide

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Technology Process of 4-{[(1'R,2'R)-1'-hydroxy-1',3'-dihydro-1H,2'H-2,2'-biinden-2'-yl]methyl}-N,N-dimethylbenzamide

There total 1 articles about 4-{[(1'R,2'R)-1'-hydroxy-1',3'-dihydro-1H,2'H-2,2'-biinden-2'-yl]methyl}-N,N-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1380445-10-2
4-(((1R,2R)-2,3-dihydro-1-hydroxy-2-(1H-inden-2-yl)-1H-inden-2-yl)methyl)benzoic acid

: 124-40-3
dimethyl amine

: 1421332-96-8
4-{[(1'R,2'R)-1'-hydroxy-1',3'-dihydro-1H,2'H-2,2'-biinden-2'-yl]methyl}-N,N-dimethylbenzamide

Guidance literature:: With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; at 20 ℃; for 12h;

Reference yield:

: 1421332-96-8
4-{[(1'R,2'R)-1'-hydroxy-1',3'-dihydro-1H,2'H-2,2'-biinden-2'-yl]methyl}-N,N-dimethylbenzamide

: 1421333-19-8
(1R,2R)-2-[4-(dimethylcarbamoyl)benzyl]-2,3-dihydro-1H,1'H-2,2'-biinden-1-yl L-leucinate

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; dmap / ethyl acetate / 12 h / 20 °C

2: dimethyl amine / tetrahydrofuran / 1 h / 0 - 20 °C

With dmap; dimethyl amine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethyl acetate;