1,8-diacetoxy-10-[(4-methoxybenzoyloxy)-4-methoxyphenylmethylene]-9(10H)-anthracenone

Base Information

• Chemical Name: 1,8-diacetoxy-10-[(4-methoxybenzoyloxy)-4-methoxyphenylmethylene]-9(10H)-anthracenone
• CAS No.: 209347-43-3
• Molecular Formula: C₃₄H₂₆O₉
• Molecular Weight: 578.575
• Mol file: 209347-43-3.mol

Synonyms:1,8-diacetoxy-10-[(4-methoxybenzoyloxy)-4-methoxyphenylmethylene]-9(10H)-anthracenone

Chemical Property of 1,8-diacetoxy-10-[(4-methoxybenzoyloxy)-4-methoxyphenylmethylene]-9(10H)-anthracenone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1,8-diacetoxy-10-[(4-methoxybenzoyloxy)-4-methoxyphenylmethylene]-9(10H)-anthracenone

There total 1 articles about 1,8-diacetoxy-10-[(4-methoxybenzoyloxy)-4-methoxyphenylmethylene]-9(10H)-anthracenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

1,8-diacetyloxy-9(10H)-anthracenone (38165-75-2) + 4-methoxy-benzoyl chloride (100-07-2) → 1,8-diacetoxy-10-[(4-methoxybenzoyloxy)-4-methoxyphenylmethylene]-9(10H)-anthracenone (209347-43-3)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1016/S0223-5234(98)80010-X

Reference yield: 58.0%

1,8-diacetoxy-10-[(4-methoxybenzoyloxy)-4-methoxyphenylmethylene]-9(10H)-anthracenone (209347-43-3) → 1-hydroxy-10-(4-methoxybenzoyl)-8-(4-methoxybenzoyloxy)-9(10H)-anthracenone

Guidance literature:

With sodium hydroxide; In methanol; Ambient temperature;

DOI:10.1016/S0223-5234(98)80010-X

Reference yield: 29.0%

1,8-diacetoxy-10-[(4-methoxybenzoyloxy)-4-methoxyphenylmethylene]-9(10H)-anthracenone (209347-43-3) → 1,8-dihydroxy-10-(4-methoxybenzoyl)-9(10H)-anthracenone

Guidance literature:

With sodium hydroxide; In methanol; Ambient temperature;

DOI:10.1016/S0223-5234(98)80010-X

upstream raw materials:

1,8-diacetyloxy-9(10H)-anthracenone

4-methoxy-benzoyl chloride