(E)-3,3-dimethyl-1,5,5-triphenyl-2-aza-1,4-pentadiene

Base Information

Chemical Name:(E)-3,3-dimethyl-1,5,5-triphenyl-2-aza-1,4-pentadiene
CAS No.:605671-70-3
Molecular Formula:C₂₄H₂₃N
Molecular Weight:325.453
Hs Code.:

Synonyms:(E)-3,3-dimethyl-1,5,5-triphenyl-2-aza-1,4-pentadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3,3-dimethyl-1,5,5-triphenyl-2-aza-1,4-pentadiene

Chemical Property:

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Technology Process of (E)-3,3-dimethyl-1,5,5-triphenyl-2-aza-1,4-pentadiene

There total 6 articles about (E)-3,3-dimethyl-1,5,5-triphenyl-2-aza-1,4-pentadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 100-52-7
benzaldehyde

: 605671-92-9
1,1-dimethyl-3,3-diphenyl-2-propenylamine

: 605671-70-3
(E)-3,3-dimethyl-1,5,5-triphenyl-2-aza-1,4-pentadiene

Guidance literature:: In diethyl ether; for 10h; Heating;
DOI:10.1021/jo034452g

Reference yield:

: 110835-94-4
2,2-dimethyl-4,4-diphenylbut-3-enoic acid

: 605671-70-3
(E)-3,3-dimethyl-1,5,5-triphenyl-2-aza-1,4-pentadiene

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂ / Heating

2: 4.9 g / sodium azide; tetrabutylammonium bromide / CH₂Cl₂; H₂O / 2 h / 0 °C

3: toluene / 4 h / Heating

4: 2.77 g / aqueous HCl / 4 h / Heating

5: 80 percent / diethyl ether / 10 h / Heating

With hydrogenchloride; thionyl chloride; sodium azide; tetrabutylammomium bromide; In diethyl ether; dichloromethane; water; toluene; 3: Curtius reaction;
DOI:10.1021/jo034452g

Reference yield:

: 492449-46-4
methyl 2,2-dimethyl-4,4-diphenyl-3-butenoate

: 605671-70-3
(E)-3,3-dimethyl-1,5,5-triphenyl-2-aza-1,4-pentadiene

Guidance literature:: Multi-step reaction with 6 steps

1: KOH / ethanol / Heating

2: SOCl₂ / Heating

3: 4.9 g / sodium azide; tetrabutylammonium bromide / CH₂Cl₂; H₂O / 2 h / 0 °C

4: toluene / 4 h / Heating

5: 2.77 g / aqueous HCl / 4 h / Heating

6: 80 percent / diethyl ether / 10 h / Heating

With hydrogenchloride; potassium hydroxide; thionyl chloride; sodium azide; tetrabutylammomium bromide; In diethyl ether; ethanol; dichloromethane; water; toluene; 4: Curtius reaction;
DOI:10.1021/jo034452g