N-methyl-4-[3-[(2R,3S,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]phenoxy]benzamide

Base Information

Chemical Name:N-methyl-4-[3-[(2R,3S,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]phenoxy]benzamide
CAS No.:1453850-82-2
Molecular Formula:C₂₀H₂₃NO₇
Molecular Weight:389.405
Hs Code.:

Synonyms:N-methyl-4-[3-[(2R,3S,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]phenoxy]benzamide

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Chemical Property of N-methyl-4-[3-[(2R,3S,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]phenoxy]benzamide

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Technology Process of N-methyl-4-[3-[(2R,3S,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]phenoxy]benzamide

There total 6 articles about N-methyl-4-[3-[(2R,3S,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]phenoxy]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1453855-78-1
((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-(4-(methylcarbamoyl)phenoxy)phenyl)tetrahydro-2H-pyran-2-yl)methyl acetate

: 1453850-82-2
N-methyl-4-[3-[(2R,3S,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]phenoxy]benzamide

Guidance literature:: With sodium methylate; In methanol; for 0.333333h;

Reference yield:

: 1453855-65-6
[(2R,3S,4R,5S,6R)-3-acetoxy-6-[3-[tert-butyl(dimethyl)silyl]oxyphenyl]-4,5-dihydroxytetrahydropyran-2-yl]methyl acetate

: 1453850-82-2
N-methyl-4-[3-[(2R,3S,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]phenoxy]benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h

2: copper diacetate; 2,6-dimethylpyridine / dichloromethane / 48 h / 20 °C / Molecular sieve

3: sodium methylate / methanol / 0.33 h

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; sodium methylate; copper diacetate; acetic acid; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 1453855-49-6
((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-hydroxyphenyl)tetrahydro-2H-pyran-2-yl)methyl acetate

: 1453850-82-2
N-methyl-4-[3-[(2R,3S,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]phenoxy]benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper diacetate; 2,6-dimethylpyridine / dichloromethane / 48 h / 20 °C / Molecular sieve

2: sodium methylate / methanol / 0.33 h

With 2,6-dimethylpyridine; sodium methylate; copper diacetate; In methanol; dichloromethane;