((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-(4-(methylcarbamoyl)phenoxy)phenyl)tetrahydro-2H-pyran-2-yl)methyl acetate

Base Information

Chemical Name:((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-(4-(methylcarbamoyl)phenoxy)phenyl)tetrahydro-2H-pyran-2-yl)methyl acetate
CAS No.:1453855-78-1
Molecular Formula:C₂₄H₂₇NO₉
Molecular Weight:473.48
Hs Code.:

Synonyms:((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-(4-(methylcarbamoyl)phenoxy)phenyl)tetrahydro-2H-pyran-2-yl)methyl acetate

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Chemical Property of ((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-(4-(methylcarbamoyl)phenoxy)phenyl)tetrahydro-2H-pyran-2-yl)methyl acetate

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Technology Process of ((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-(4-(methylcarbamoyl)phenoxy)phenyl)tetrahydro-2H-pyran-2-yl)methyl acetate

There total 5 articles about ((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-(4-(methylcarbamoyl)phenoxy)phenyl)tetrahydro-2H-pyran-2-yl)methyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [4-(methylcarbamoyl)phenyl]boronic acid

: 1453855-49-6
((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-hydroxyphenyl)tetrahydro-2H-pyran-2-yl)methyl acetate

: 1453855-78-1
((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-(4-(methylcarbamoyl)phenoxy)phenyl)tetrahydro-2H-pyran-2-yl)methyl acetate

Guidance literature:: With 2,6-dimethylpyridine; copper diacetate; In dichloromethane; at 20 ℃; for 48h; Molecular sieve;

Reference yield:

: 1453855-65-6
[(2R,3S,4R,5S,6R)-3-acetoxy-6-[3-[tert-butyl(dimethyl)silyl]oxyphenyl]-4,5-dihydroxytetrahydropyran-2-yl]methyl acetate

: 1453855-78-1
((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-(4-(methylcarbamoyl)phenoxy)phenyl)tetrahydro-2H-pyran-2-yl)methyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h

2: copper diacetate; 2,6-dimethylpyridine / dichloromethane / 48 h / 20 °C / Molecular sieve

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; copper diacetate; acetic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 2873-29-2
D-glucal triacetate

: 1453855-78-1
((2R,3S,4R,5S,6R)-3-acetoxy-4,5-dihydroxy-6-(3-(4-(methylcarbamoyl)phenoxy)phenyl)tetrahydro-2H-pyran-2-yl)methyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: palladium diacetate / acetonitrile / 20 °C

2: 4-methylmorpholine N-oxide; methanesulfonamide; osmium(VIII) oxide; 2,6-dimethylpyridine / water; tert-butyl alcohol / 20 °C

3: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h

4: copper diacetate; 2,6-dimethylpyridine / dichloromethane / 48 h / 20 °C / Molecular sieve

With 2,6-dimethylpyridine; osmium(VIII) oxide; methanesulfonamide; tetrabutyl ammonium fluoride; copper diacetate; palladium diacetate; acetic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; water; acetonitrile; tert-butyl alcohol;