6-methoxy-1-(3,4-methylenedioxyphenyl)methyl-2-oxo-3-phenylsulfanyl-2,3-dihydroindole

Base Information

Chemical Name:6-methoxy-1-(3,4-methylenedioxyphenyl)methyl-2-oxo-3-phenylsulfanyl-2,3-dihydroindole
CAS No.:374593-84-7
Molecular Formula:C₂₃H₁₉NO₄S
Molecular Weight:405.474
Hs Code.:

Synonyms:6-methoxy-1-(3,4-methylenedioxyphenyl)methyl-2-oxo-3-phenylsulfanyl-2,3-dihydroindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methoxy-1-(3,4-methylenedioxyphenyl)methyl-2-oxo-3-phenylsulfanyl-2,3-dihydroindole

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Technology Process of 6-methoxy-1-(3,4-methylenedioxyphenyl)methyl-2-oxo-3-phenylsulfanyl-2,3-dihydroindole

There total 7 articles about 6-methoxy-1-(3,4-methylenedioxyphenyl)methyl-2-oxo-3-phenylsulfanyl-2,3-dihydroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 374593-79-0
N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfinylacetamide

: 374593-84-7
6-methoxy-1-(3,4-methylenedioxyphenyl)methyl-2-oxo-3-phenylsulfanyl-2,3-dihydroindole

Guidance literature:: With trifluoroacetic anhydride; In benzene; at 20 ℃; for 1h;
DOI:10.1248/cpb.49.1132

Reference yield:

: 7031-27-8
(phenylthio)acetic acid chloride

: 374593-84-7
6-methoxy-1-(3,4-methylenedioxyphenyl)methyl-2-oxo-3-phenylsulfanyl-2,3-dihydroindole

Guidance literature:: Multi-step reaction with 3 steps

1: 22.6 g / Et₃N / benzene / 20 h / 20 °C

2: 99 percent / NaIO₄ / methanol; H₂O / 2 h / Heating

3: 99 percent / TFAA / benzene / 1 h / 20 °C

With sodium periodate; triethylamine; trifluoroacetic anhydride; In methanol; water; benzene; 3: Pummerer reaction;
DOI:10.1248/cpb.49.1132

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 374593-84-7
6-methoxy-1-(3,4-methylenedioxyphenyl)methyl-2-oxo-3-phenylsulfanyl-2,3-dihydroindole

Guidance literature:: Multi-step reaction with 4 steps

1.1: Ti(i-PrO)4 / 3 h / 80 °C

1.2: 99 percent / NaBH₄ / methanol / 1 h / 20 °C

2.1: 22.6 g / Et₃N / benzene / 20 h / 20 °C

3.1: 99 percent / NaIO₄ / methanol; H₂O / 2 h / Heating

4.1: 99 percent / TFAA / benzene / 1 h / 20 °C

With titanium(IV) isopropylate; sodium periodate; triethylamine; trifluoroacetic anhydride; In methanol; water; benzene; 4.1: Pummerer reaction;
DOI:10.1248/cpb.49.1132